PřF:C6250 Methods of Chem. Res. - lab.

C6250 Methods of Chemical Research - laboratory

Faculty of Science
Spring 2014

Extent and Intensity

0/0/5. 5 credit(s) (plus extra credits for completion). Type of Completion: graded credit.

Teacher(s)

Guaranteed by

Timetable of Seminar Groups

C6250/01: Mon 8:00–12:50 C10/209, M. Farková
C6250/02: Mon 14:00–18:50 C10/209, A. Hrdlička
C6250/03: Tue 9:00–13:50 C10/209, M. Farková

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

Course objectives

At the end of the course students will know instrumental methods and will be able to process results of the measurements.

Syllabus

1. Orientation tests, qualitative elemental analysis, classification and group reactions, physical constants determination of organic compounds. 2. Semimicrodetermination of carbon and hydrogen. 3. Volumetric determination of nitrogen according to Dumas and Dubsky. 4. Microdetermination of sulfur according to Schöniger. 5. Derivatization of alcohols and their identification by TLC. 6. Interpretation of spectra of organic molecules. 7. Gas chromatography. Determination of alcohols in an alcoholic drink. 8. Capillary electrophoresis. Determination of caffeine and acetylsalicylic acid in Acylcoffin. 9. Liquid chromatography on reverse phase with UV-VIS detection

Literature

STRÁNSKÝ, Zdeněk. Analýza organických sloučenin. 1. vyd. Olomouc: Univerzita Palackého. 235 s. 1981. info
STRÁNSKÝ, Zdeněk. Analýza organických sloučenin b. 1. vyd. Olomouc: Univerzita Palackého. 235 s. 1981. info

Teaching methods

Type of education: students have to pass all exercises included in the course

Assessment methods

Type of exam: written tests, final test, oral examination during the lessons. Students have to submit all protocols.

Language of instruction

Czech

Further Comments

Study Materials
Course is no more offered.