C7998 Basics of Experimental NMR Spectroscopy

Faculty of Science
Spring 2009
Extent and Intensity
0/0/1. 1 credit(s). Type of Completion: z (credit).
Teacher(s)
Mgr. Kateřina Bouzková, Ph.D. (seminar tutor)
RNDr. Otakar Humpa (seminar tutor)
prof. RNDr. Radek Marek, Ph.D. (seminar tutor)
Guaranteed by
prof. RNDr. Radek Marek, Ph.D.
National Centre for Biomolecular Research – Faculty of Science
Prerequisites
Basic knowledge of NMR spectroscopy.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
Course objectives
Measurements of 1D NMR spectra (1H, 13C, APT) with 300 MHz spectrometer; replacement of probeheadů temperature control; data processing; interpretation of the spectra; file transfer.
The course is aimed for controlling the high-resolution NMR spectrometer (1H and 13C spectra, alternatively 31P and 19F).
Syllabus
  • 1. NMR spectrometer, TopSpin software, probehead, NMR tube, sample preparation, 1H NMR spectra. 2. Data processing, temperature unit, 13C NMR, APT experiment. 3. Replacement of probehead, ACD software, interpretation of spectra, various isotopes - experimental aspects. File transfer.
Literature
  • Claridge, Timothy D.W. High-Resolution NMR Techniques in Organic Chemistry, Amsterdam, Pergamon, 1999, ISBN 0-08-042798-7
  • Braun, S. - Kalinowski, H.O. - Berger, S. 100 and More Basic NMR Experiments, Weinheim, VCH, 1996, ISBN 3-527-29091-5
Assessment methods
Practical sessions. Practical exam.
Language of instruction
Czech
Follow-Up Courses
Further Comments
The course is taught each semester.
The course is taught: in blocks.
Teacher's information
http://www.chemi.muni.cz/nmr/radek/C7998/
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Autumn 2010 - only for the accreditation, Autumn 2006, Spring 2007, Autumn 2007, Spring 2008, Autumn 2008, Autumn 2009, Spring 2010, Autumn 2010, Spring 2011, Autumn 2011, Autumn 2011 - acreditation, spring 2012 - acreditation, Autumn 2012, Autumn 2013, Autumn 2014, Autumn 2015, Spring 2016, Autumn 2016, Spring 2017, autumn 2017, spring 2018, Autumn 2018, Spring 2019, Autumn 2019, Spring 2020, Autumn 2020, Spring 2021, autumn 2021, Spring 2022, Autumn 2022, Spring 2023, Autumn 2023, Spring 2024, Autumn 2024, Spring 2025.
  • Enrolment Statistics (Spring 2009, recent)
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