C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2009
Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: graded credit.
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Timetable
Tue 8:00–11:50 C10/312
Prerequisites
NOW ( C7777 Handling chemicals )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 17 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2008
Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: graded credit.
Teacher(s)
RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Stanislav Man, Ph.D. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
Mgr. Zdeněk Spíchal, Ph.D. (seminar tutor)
Světlana Filípková (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Timetable of Seminar Groups
C1080/01: Tue 16:00–19:50 C10/312, M. Černík
C1080/02: Wed 12:00–15:50 C10/312, M. Černík
C1080/03: Thu 12:00–15:50 C10/312, A. Pálková
C1080/04: Mon 13:00–16:50 C10/312, A. Pálková
C1080/05: Thu 16:00–19:50 C10/312, S. Man
C1080/06: Thu 8:00–11:50 C10/312, A. Pálková
C1080/07: Fri 8:00–11:50 C10/312, J. Pinkas
C1080/08: Wed 16:00–19:50 C10/312, J. Pinkas
C1080/09: Tue 12:00–15:50 C10/312, A. Pálková
C1080/10: Tue 8:00–11:50 C10/312, Z. Spíchal
Prerequisites
NOW ( C7777 Handling chemicals )
Theoretical knowledge and practicla skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 24 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2007
Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: graded credit.
Teacher(s)
RNDr. Miloš Černík, CSc. (seminar tutor)
Ing. Jitka Halvová (seminar tutor)
Mgr. Jiří Křivohlávek (seminar tutor)
Ing. Blanka Vrbková, Ph.D. (seminar tutor)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Timetable of Seminar Groups
C1080/01: Tue 16:00–19:50 C10/312, M. Černík
C1080/02: Thu 8:00–11:50 C10/312, M. Černík
C1080/03: Thu 12:00–15:50 C10/312, J. Křivohlávek
C1080/04: Fri 7:00–10:50 C10/312, J. Křivohlávek
C1080/05: Tue 8:00–11:50 C10/312, J. Křivohlávek
C1080/06: Fri 12:00–15:50 C10/312, J. Křivohlávek
C1080/07: Wed 12:00–15:50 C10/312, J. Halvová
C1080/08: Wed 16:00–19:50 C10/312, B. Vrbková
C1080/09: Tue 12:00–15:50 C10/312, J. Halvová
C1080/10: Thu 16:00–19:50 C10/312, J. Křivohlávek
Prerequisites
Theoretical knowledge and practicla skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 24 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations(filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, sublimation, drying, extraction, thin layer chromatography. Measurement, precision, accuracy, significant figures. Gas and liquid volume measurements. Balances and weighing. Density, refractive index, melting point.

    3. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner.

    4. Experiment 1, part 1. Filtration, vacuum filtration, distillation, liquid volume measurements, pipette, burette, preparation of a solution with precise concentration, concentration calculations.

    5. Experiment 2.

    6. Experiment 3. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    7. Experiment 4. Distillation of HCl.

Literature
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Assessment methods (in Czech)
Laboratorní cvičení probíhá každý týden. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena a pro získání klasifikovaného zápočtu je nutno je nahradit do konce semestru.
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course can also be completed outside the examination period.
The course is taught annually.
General note: Vyučují učitelé katedry anorganické chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2006
Extent and Intensity
0/4/0. 4 credit(s) (fasci plus compl plus > 4). Type of Completion: graded credit.
Teacher(s)
RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
Mgr. Jiří Křivohlávek (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
prof. RNDr. Jiří Příhoda, CSc. (seminar tutor)
RNDr. Jan Taraba, Ph.D. (seminar tutor)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Timetable of Seminar Groups
C1080/01: Thu 8:00–11:50 03016, J. Křivohlávek
C1080/02: Mon 14:00–17:50 03016, D. Dastych
C1080/03: Tue 12:00–15:50 03016, D. Dastych
C1080/04: Tue 16:00–19:50 03016, D. Dastych
C1080/05: Fri 11:00–14:50 03016, J. Křivohlávek
C1080/06: Wed 12:00–15:50 03016, J. Taraba
C1080/07: Wed 16:00–19:50 03016, J. Taraba
C1080/08: Tue 7:00–10:50 03016, M. Černík
C1080/09: Wed 7:00–10:50 03016, M. Černík
C1080/10: Fri 15:00–18:50 03016, J. Novosad
C1080/11: Fri 7:00–10:50 03016, J. Křivohlávek
C1080/12: Thu 16:00–19:50 03016, J. Pinkas
C1080/13: No timetable has been entered into IS.
Prerequisites
Theoretical knowledge and practicla skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 24 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations(filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, sublimation, drying, extraction, thin layer chromatography. Measurement, precision, accuracy, significant figures. Gas and liquid volume measurements. Balances and weighing. Density, refractive index, melting point.

    3. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner.

    4. Experiment 1, part 1. Filtration, vacuum filtration, distillation, liquid volume measurements, pipette, burette, preparation of a solution with precise concentration, concentration calculations.

    5. Experiment 2.

    6. Experiment 3. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    7. Experiment 4. Distillation of HCl.

Literature
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Assessment methods (in Czech)
Laboratorní cvičení probíhá každý týden. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena a pro získání klasifikovaného zápočtu je nutno je nahradit do konce semestru.
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course can also be completed outside the examination period.
The course is taught annually.
General note: Vyučují učitelé katedry anorganické chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2005
Extent and Intensity
0/4/0. 3 credit(s). Type of Completion: graded credit.
Teacher(s)
RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
Mgr. Jiří Křivohlávek (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
prof. RNDr. Jiří Příhoda, CSc. (seminar tutor)
RNDr. Jan Taraba, Ph.D. (seminar tutor)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Timetable of Seminar Groups
C1080/03: Tue 12:00–15:50 03016, M. Černík
C1080/07: Tue 16:00–19:50 03016, J. Křivohlávek
C1080/04: Wed 8:00–11:50 03016, J. Taraba
C1080/09: Wed 16:00–19:50 03016, J. Křivohlávek
C1080/10: Thu 7:00–10:50 03016, M. Černík
C1080/06: Thu 12:00–15:50 03016, J. Příhoda
C1080/08: Thu 16:00–19:50 03016, J. Křivohlávek
C1080/02: Fri 7:00–10:50 03016, D. Dastych
C1080/05: Fri 11:00–14:50 03016, J. Taraba
C1080/01: Fri 15:00–18:50 03016, J. Novosad
Prerequisites
Theoretical knowledge and practicla skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 24 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations(filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, sublimation, drying, extraction, thin layer chromatography. Measurement, precision, accuracy, significant figures. Gas and liquid volume measurements. Balances and weighing. Density, refractive index, melting point.

    3. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner.

    4. Experiment 1, part 1. Filtration, vacuum filtration, distillation, liquid volume measurements, pipette, burette, preparation of a solution with precise concentration, concentration calculations.

    5. Experiment 2.

    6. Experiment 3. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    7. Experiment 4. Distillation of HCl.

Literature
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Assessment methods (in Czech)
Laboratorní cvičení probíhá každý týden. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena a pro získání klasifikovaného zápočtu je nutno je nahradit do konce semestru.
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course can also be completed outside the examination period.
The course is taught annually.
General note: Vyučují učitelé katedry anorganické chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2004
Extent and Intensity
0/4/0. 3 credit(s). Type of Completion: graded credit.
Teacher(s)
RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
Mgr. Jiří Křivohlávek (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
prof. RNDr. Jiří Příhoda, CSc. (seminar tutor)
RNDr. Jan Taraba, Ph.D. (seminar tutor)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Timetable of Seminar Groups
C1080/01: Thu 16:00–19:50 03016, J. Pinkas
C1080/02: Wed 15:00–18:50 03016, J. Taraba
C1080/03: Thu 12:00–15:50 03016, D. Dastych
C1080/04: Tue 12:00–15:50 03016, D. Dastych
C1080/05: Wed 7:00–10:50 03016, M. Černík
C1080/06: Tue 16:00–19:50 03016, J. Křivohlávek
C1080/07: Fri 7:00–10:50 03016, J. Příhoda
C1080/08: Fri 11:00–14:50 03016, J. Křivohlávek
C1080/09: Thu 7:00–10:50 03016, J. Taraba
Prerequisites
Theoretical knowledge and practicla skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 24 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations(filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, sublimation, drying, extraction, thin layer chromatography. Measurement, precision, accuracy, significant figures. Gas and liquid volume measurements. Balances and weighing. Density, refractive index, melting point.

    3. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner.

    4. Experiment 1, part 1. Filtration, vacuum filtration, distillation, liquid volume measurements, pipette, burette, preparation of a solution with precise concentration, concentration calculations.

    5. Experiment 2.

    6. Experiment 3. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    7. Experiment 4. Distillation of HCl.

Literature
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Assessment methods (in Czech)
Laboratorní cvičení probíhá každý týden. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena a pro získání klasifikovaného zápočtu je nutno je nahradit do konce semestru.
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
Study Materials
The course can also be completed outside the examination period.
The course is taught annually.
General note: Vyučují učitelé katedry anorganické chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2003
Extent and Intensity
0/2/0. 3 credit(s). Type of Completion: graded credit.
Teacher(s)
RNDr. Milan Alberti, CSc. (seminar tutor)
RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
Mgr. Jiří Křivohlávek (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
prof. RNDr. Jiří Příhoda, CSc. (seminar tutor)
RNDr. Jan Taraba, Ph.D. (seminar tutor)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Timetable of Seminar Groups
C1080/01: No timetable has been entered into IS. D. Dastych
C1080/01a: No timetable has been entered into IS. D. Dastych
C1080/02: No timetable has been entered into IS. J. Taraba
C1080/02a: No timetable has been entered into IS. J. Taraba
C1080/03: No timetable has been entered into IS. D. Dastych
C1080/03a: No timetable has been entered into IS. D. Dastych
C1080/04: No timetable has been entered into IS. M. Černík
C1080/04a: No timetable has been entered into IS. M. Černík
C1080/05: No timetable has been entered into IS. J. Příhoda
C1080/05a: No timetable has been entered into IS. J. Příhoda
Prerequisites
Theoretical knowledge and practicla skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 24 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations(filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, sublimation, drying, extraction, thin layer chromatography. Measurement, precision, accuracy, significant figures. Gas and liquid volume measurements. Balances and weighing. Density, refractive index, melting point.

    3. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner.

    4. Experiment 1, part 1. Filtration, vacuum filtration, distillation, liquid volume measurements, pipette, burette, preparation of a solution with precise concentration, concentration calculations.

    5. Experiment 2.

    6. Experiment 3. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    7. Experiment 4. Distillation of HCl.

Literature
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Assessment methods (in Czech)
Laboratorní cvičení probíhá každý týden. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena a pro získání klasifikovaného zápočtu je nutno je nahradit do konce semestru.
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course can also be completed outside the examination period.
The course is taught annually.
General note: Vyučují učitelé katedry anorganické chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2002
Extent and Intensity
0/0/5. 3 credit(s). Type of Completion: graded credit.
Teacher(s)
RNDr. Milan Alberti, CSc. (seminar tutor)
RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
Mgr. Jiří Křivohlávek (seminar tutor)
RNDr. Aleš Mareček, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
prof. RNDr. Jiří Příhoda, CSc. (seminar tutor)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Timetable of Seminar Groups
C1080/01: No timetable has been entered into IS. M. Nečas
C1080/02: No timetable has been entered into IS. M. Nečas
C1080/03: No timetable has been entered into IS. M. Nečas
C1080/04: No timetable has been entered into IS. D. Dastych
C1080/05: No timetable has been entered into IS. D. Dastych
C1080/06: No timetable has been entered into IS. J. Křivohlávek
C1080/07: No timetable has been entered into IS. J. Křivohlávek
C1080/08: No timetable has been entered into IS. J. Křivohlávek
C1080/09: No timetable has been entered into IS. M. Černík
Prerequisites
Theoretical knowledge and practicla skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 24 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations(filtration, crystallization, distillation, rectification, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, sublimation, drying, extraction, thin layer chromatography. Measurement, precision, accuracy, significant figures. Gas and liquid volume measurements. Balances and weighing. Density, refractive index, melting point.

    3. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner.

    4. Experiment 1, part 1. Filtration, vacuum filtration, distillation, liquid volume measurements, pipette, burette, preparation of a solution with precise concentration, concentration calculations.

    5. Experiment 1, part 2. Vacuum distillation, rectification, Soxhlet extraction, sublimation. Melting point, refractive index. Rotary evaporator. Heating under reflux.

    6. Experiment 2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    7. Experiment 3. Volumetric measurements of the molar mass of Mg a Al.

    8. Experiment 4. Distillation of HCl.

    9. Experiment 5. Clove extract, TLC, Experiment 11. Melting point measurement.

    10. Experiment 6. Acetone + toluene distillation, Experiment 10. VSEPR.

    11. Experiment 7. Acetone + toluene rectification.

    12. Experiment 8. Electrode potentials.

    13. Experiment 9. Vacuum distillation.

    14. Final test, glassware and lab cleaning.
Literature
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Assessment methods (in Czech)
Laboratorní cvičení probíhá každý týden. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena a pro získání klasifikovaného zápočtu je nutno je nahradit do konce semestru.
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course can also be completed outside the examination period.
The course is taught annually.
General note: Vyučují učitelé katedry anorganické chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2001
Extent and Intensity
0/5/0. 6 credit(s). Type of Completion: graded credit.
Teacher(s)
RNDr. Milan Alberti, CSc. (seminar tutor)
RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
RNDr. Aleš Mareček, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
prof. RNDr. Jiří Příhoda, CSc. (seminar tutor)
Guaranteed by
doc. RNDr. Josef Novosad, CSc.
Chemistry Section – Faculty of Science
Course Enrolment Limitations
The course is only offered to the students of the study fields the course is directly associated with.
fields of study / plans the course is directly associated with
there are 24 fields of study the course is directly associated with, display
Course objectives
Basic laboratory work (filtration, crystallization, precipitation, distillation, rectification, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised.
Syllabus (in Czech)
  • 1. Úvod do cvičení, seznámení posluchačů s vybavením Organizace práce ve cvičení - laboratorní řád, pokyny pro vypracování protokolů. Bezpečnost práce v chemické laboratoři: Požadavky pro udělení zápočtu. Chemikálie. Tlakové láhve. Laboratorní sklo a keramika Kovy, plasty, guma, papír. Zahřívání, chlazení, míchání. Prostá destilace, frakční destilace.

    2. Měření tlaku, zdroje vakua. Rektifikace, destilace za sníženého tlaku, sublimace, sušení, extrakce, vytřepávání, tenkovrstvá chromatografie. Měření, přesnost, správnost, platné číslice. Měření objemu kapalin a plynů. Váhy a vážení. Stanovení hustoty, indexu lomu, bodu tání.

    3. Sklofoukačské práce, ukázka práce kvalifikovaného skláře, vlastní práce na sklářském kahanu, práce se sklem na Bunsenově kahanu.

    4. Úloha č. 1, první část. Filtrace, vakuová filtrace, prostá destilace, měření objemů kapalin pipetou a byretou, příprava odměrného roztoku, výpočet koncentrace roztoku.

    5. Úloha č. 1, druhá část. Vakuová destilace, rektifikace, extrakce na Soxhletově přístroji, sublimace a vytřepávání. Teplota tání, index lomu, vakuová odparka, zahřívání pod zpětným chladičem.

    6. Úloha č. 2. Dělení směsi KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3

    7. Úloha č. 3. Stanovení Mr Mg a Al

    8. Úloha č. 4. Destilace HCl

    9. Úloha č. 5. Hřebíčková silice, Úloha č. 11. Stanovení bodu tání

    10. Úloha č. 6. Aceton + toluen jednoduchá destilace, Úloha č. 10. VSEPR

    11. Úloha č. 7. Aceton + toluen rektifikace

    12. Úloha č. 8. Elektrodové potenciály

    13. Úloha č. 9. Destilace za sníženého tlaku

    14. Zápočtová písemná práce, úklid laboratoře.
Language of instruction
Czech
Further comments (probably available only in Czech)
The course can also be completed outside the examination period.
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé katedry anorganické chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2000
Extent and Intensity
0/5/0. 6 credit(s). Type of Completion: graded credit.
Teacher(s)
RNDr. Milan Alberti, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
Mgr. Vojtěch Jančík, Ph.D. (seminar tutor)
RNDr. Aleš Mareček, CSc. (seminar tutor)
doc. Mgr. Marek Nečas, Ph.D. (seminar tutor)
Mgr. Věra Novoměstská, Ph.D. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
doc. RNDr. Antonín Růžička, CSc. (seminar tutor)
Guaranteed by
doc. RNDr. Josef Novosad, CSc.
Chemistry Section – Faculty of Science
Course Enrolment Limitations
The course is only offered to the students of the study fields the course is directly associated with.
fields of study / plans the course is directly associated with
there are 24 fields of study the course is directly associated with, display
Course objectives
Basic laboratory work (filtration, crystallization, precipitation, distillation, rectification, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised.
Language of instruction
Czech
Further comments (probably available only in Czech)
The course can also be completed outside the examination period.
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé katedry anorganické chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 1999
Extent and Intensity
0/5/0. 6 credit(s). Type of Completion: graded credit.
Teacher(s)
RNDr. Milan Alberti, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
RNDr. Aleš Mareček, CSc. (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
prof. RNDr. Jiří Příhoda, CSc. (seminar tutor)
doc. RNDr. Antonín Růžička, CSc. (seminar tutor)
Guaranteed by
doc. RNDr. Josef Novosad, CSc.
Chemistry Section – Faculty of Science
Course Enrolment Limitations
The course is only offered to the students of the study fields the course is directly associated with.
fields of study / plans the course is directly associated with
there are 26 fields of study the course is directly associated with, display
Syllabus
  • Basic laboratory work (filtration, crystallization, precipitation, distillation, rectification, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised.
Language of instruction
Czech
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Ve studijních programech 1407R a 1407T nutno zapsat a úspěšně zakončit v prvním semestru studia. Vyučují učitelé katedry anorganické chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2024

The course is not taught in Autumn 2024

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: z (credit).
Taught in person.
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Prerequisites
NOW ( C7777 Handling chemical substances )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2023

The course is not taught in Autumn 2023

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: z (credit).
Taught in person.
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Prerequisites
NOW ( C7777 Handling chemical substances )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2022

The course is not taught in Autumn 2022

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: z (credit).
Taught in person.
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Prerequisites
NOW ( C7777 Handling chemical substances )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
autumn 2021

The course is not taught in autumn 2021

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: z (credit).
Taught in person.
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Prerequisites
NOW ( C7777 Handling chemical substances )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2020

The course is not taught in Autumn 2020

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: z (credit).
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Prerequisites
NOW ( C7777 Handling chemicals )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2019

The course is not taught in Autumn 2019

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: z (credit).
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Prerequisites
NOW ( C7777 Handling chemicals )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2018

The course is not taught in Autumn 2018

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: z (credit).
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Prerequisites
NOW ( C7777 Handling chemicals )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
autumn 2017

The course is not taught in autumn 2017

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: graded credit.
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Prerequisites
NOW ( C7777 Handling chemicals )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2016

The course is not taught in Autumn 2016

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: graded credit.
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Prerequisites
NOW ( C7777 Handling chemicals )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2015

The course is not taught in Autumn 2015

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: graded credit.
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Prerequisites
NOW ( C7777 Handling chemicals )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2014

The course is not taught in Autumn 2014

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: graded credit.
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Prerequisites
NOW ( C7777 Handling chemicals )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2013

The course is not taught in Autumn 2013

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: graded credit.
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Prerequisites
NOW ( C7777 Handling chemicals )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2012

The course is not taught in Autumn 2012

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: graded credit.
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Supplier department: Department of Chemistry – Chemistry Section – Faculty of Science
Prerequisites
NOW ( C7777 Handling chemicals )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2011

The course is not taught in Autumn 2011

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: graded credit.
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Prerequisites
NOW ( C7777 Handling chemicals )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2010

The course is not taught in Autumn 2010

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: graded credit.
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Prerequisites
NOW ( C7777 Handling chemicals )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2007 - for the purpose of the accreditation
Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: graded credit.
Teacher(s)
RNDr. Miloš Černík, CSc. (seminar tutor)
RNDr. Dalibor Dastych, Dr. (seminar tutor)
RNDr. Marta Farková, CSc. (seminar tutor)
Mgr. Jiří Křivohlávek (seminar tutor)
doc. RNDr. Josef Novosad, CSc. (seminar tutor)
Ing. Alena Pálková (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
prof. RNDr. Jiří Příhoda, CSc. (seminar tutor)
RNDr. Jan Taraba, Ph.D. (seminar tutor)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Prerequisites
Theoretical knowledge and practicla skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 24 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations(filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, sublimation, drying, extraction, thin layer chromatography. Measurement, precision, accuracy, significant figures. Gas and liquid volume measurements. Balances and weighing. Density, refractive index, melting point.

    3. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner.

    4. Experiment 1, part 1. Filtration, vacuum filtration, distillation, liquid volume measurements, pipette, burette, preparation of a solution with precise concentration, concentration calculations.

    5. Experiment 2.

    6. Experiment 3. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    7. Experiment 4. Distillation of HCl.

Literature
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Assessment methods (in Czech)
Laboratorní cvičení probíhá každý týden. Připravenost každého posluchače na příslušnou úlohu laboratorního cvičení je kontrolována před zahájením cvičení krátkým písemným testem nebo ústním přezkoušením. Všechny výpočty pro danou úlohu musí mít posluchači připraveny v laboratorním deníku před zahájením cvičení. Zameškaná cvičení musí být řádně omluvena a pro získání klasifikovaného zápočtu je nutno je nahradit do konce semestru.
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course can also be completed outside the examination period.
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé katedry anorganické chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2011 - acreditation

The course is not taught in Autumn 2011 - acreditation

The information about the term Autumn 2011 - acreditation is not made public

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: graded credit.
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Prerequisites
NOW ( C7777 Handling chemicals )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.

C1080 General Chemistry - laboratory course

Faculty of Science
Autumn 2010 - only for the accreditation

The course is not taught in Autumn 2010 - only for the accreditation

Extent and Intensity
0/4/0. 4 credit(s). Type of Completion: graded credit.
Teacher(s)
Ing. Alena Pálková (seminar tutor)
Světlana Filípková (assistant)
doc. RNDr. Josef Novosad, CSc. (assistant)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Prerequisites
NOW ( C7777 Handling chemicals )
Theoretical knowledge and practical skills of the high school chemistry level. Writing chemical equations, stoichiometric calculations, and calculations of solution concentration and mixing.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 15 fields of study the course is directly associated with, display
Course objectives
Basic laboratory operations (filtration, crystallization, distillation, sublimation, volumetric methods) as well as determination of physicochemical constants of compounds are exercised in this course.
Students will learn in this course:
safety and fire rules and basic rules for safe chemical laboratory practice
physico-chemical measurements, operation with instruments, and evaluation of obtained data
to perform basic laboratory operations and manipulation with chemical laboratory equipment and simple instruments
to carry out more advanced laboratory experiments, data evaluation, construction of tables, graphs, and diagrams
Syllabus
  • 1. Introduction, laboratory and equipment, guidelines for lab work and writing reports, safety rules. Pass-requirements. Chemicals. Gas cylinders. Laboratory glassware and ceramics. Metal, plastic, paper. Heating, cooling, stirring. Simple distillation, fractional distillation.

    2. Glass-blowing exercise, demonstration of glassblower work, work on glassblower burner and Bunsen burner. Practical experiments: Filtration, vacuum filtration, filtration at elevated temperature.

    3. Pressure measurements, sources of vacuum. Rectification, vacuum distillation, steam-distillation. Measurement, precision, accuracy, significant figures. Practical experiments: distillation.

    4. Sublimation, drying, extraction, thin layer chromatography, refractive index, melting point. Practical experiments: melting point measurements, refractive index measurements on refractometer, extraction with Soxhlet apparatus, separation funnel, thin layer chromatography.

    5. Gas and liquid volume measurements, pipette, burette. Balances and weighing. Density and concentration calculations. Titrations. Practical experiments: preparation of a solution with precise concentration, weighing, concentration calculations.

    6. Practical experiments in groups: vacuum distillation, rectification, sublimation, rotavapor, reflux.

    7. Experiment no.2. Separation of the KAl(SO4)2.12H2O + CuSO4.5H2O + Cr2O3 mixture.

    8. Experiment no.4. Distillation of HCl. Titrations.

    9. Experiment no.3. Measurements of atomic masses of magnesium and aluminum.

    10. Experiment no.5 Isolation of eugenol from cloves by steam-distillation.

    11. Experiment no.6 Distillation of acetone+toluene mixture and construction of phase diagram.

    12. Experiment no.7 Distillation of acetone+toluene mixture with rectification column.

    13. Experiment no.9 Vacuum distillation and measurements of vapor pressure of water and ethanol as a function of temperature.

    14. Make-up class, final test.

Literature
  • NOVÁČEK, Eduard and Milan POTÁČEK. Laboratorní technika ke cvičení z metod organické chemie. Edited by Slávka Janků. 1. vyd. Brno: Masarykova univerzita, 1997, 91 s. ISBN 8021015004. info
  • Laboratorní technika a cvičení z anorganické chemie. 7. přeprac. vyd. Brno: Masarykova univerzita, 1995, 114 s. ISBN 8021010126. info
Teaching methods
Laboratory course covers basic laboratory operations and writing laboratory reports.
Assessment methods
The laboratory course runs on a weekly basis. Each student is tested at the beginning of the class for the theoretical knowledge of the particular experiment by a short written test or by questions. All calculations for the particular experiment must be performed before the class. The absence at the class must be justified by a medical report. All missed classes must be made-up by the end of the semester. Requirements for passing the class:

a) attendance at all laboratory classes (missed classes must be made-up)

b) knowledge of principles of all experiments covered in the course, stoichiometric and concentration calculations and titration evaluation

c) careful preparation and timely submission of lab reports for all experiments

d) passed test from laboratory safety rules, calculations, and experiment principles

e) paid balance for broken glassware and equipment
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
General note: Vyučují učitelé Ústavu chemie.
Listed among pre-requisites of other courses
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009.
  • Enrolment Statistics (recent)