FaF:FAAI1_15 Analytical Chemistry I - Informace o předmětu

FAAI1_15 Analytical Chemistry I

Rozsah

2/3/0. 4 kr. Ukončení: z.
Vyučováno kontaktně

Vyučující

doc. RNDr. Bc. Jiří Pazourek, Ph.D. (přednášející)
doc. RNDr. Bc. Jiří Pazourek, Ph.D. (cvičící)
Mgr. Tomáš Crha (cvičící)
Ing. Klára Odehnalová, Ph.D. (cvičící)
Bc. Gabriela Jelínková (pomocník)

Garance

doc. RNDr. Bc. Jiří Pazourek, Ph.D.
Ústav chemických léčiv – Ústavy – Farmaceutická fakulta
Kontaktní osoba: Mgr. Tereza Jůnová

Rozvrh

Čt 11:50–13:30 44-247

• Rozvrh seminárních/paralelních skupin:

FAAI1_15/01: každý lichý čtvrtek 13:30–18:30 44-339, T. Crha, K. Odehnalová, J. Pazourek

Předpoklady

STUDIJNI_SKUPINA(start_before_2025)

Omezení zápisu do předmětu

Předmět je určen pouze studentům mateřských oborů.

Mateřské obory/plány

• Multidisciplinární studia na farmaceutické fakultě (program CST, KOS)
• Pharmacy (program FaF, M-FARMA)

Anotace

Objective of the course - aims of the course unit: To provide theoretical and practical knowledge for qualified chemical and instrumental analysis of inorganic and organic substances, including drugs, emphasizing the importance of methods in drug analysis and studying structural and physicochemical properties of substances related to their biological effect. Emphasis is placed on the formation of logical thought processes of the pharmacist important for his future professional application. In practical exercises, mastering work habits and independent approach of students to solving analytical problems is consistently required.

Výstupy z učení

After completing the course, the student will be able to: - understand the meaning and principles of classical and modern analytical chemistry - have an overview of methods of qualitative analytical chemistry - practically perform basic laboratory tests of qualitative analytical chemistry

Klíčová témata

Content of the lectures 1.-3. Analytical chemistry: The goal and basic terms of the science, methods. Analytical reactions: protolytic, redox, precipitation and complexation reactions. Importance of pH. Qualitative analysis of inorganic compounds. Group reactions of cations. Group reactions of anions. Selective and specific reactions of selected pharmaceutically important ions. 4.-5. Qualitative analysis of organic compounds. Classical proofs and identification. Preliminary test. Classes of solubility. Elemental analysis. Identification of organic compounds: Proofs of functional groups. Determination of basic physical constants, precise measurement of pH. 6.-9. Qualitative analysis of organic compounds. Instrumental methods of structure analysis UV-VIS, IR, examples 10.-12. Qualitative analysis of organic compounds. Instrumental methods of structure analysis NMR, MS, examples Content of the laboratory exercises 1.+2. Organization of the exercises. Safety rules in the chemical laboratory. Group and selective reactions of cations: group reagents HCl, NaOH, NH3. Analysis of an unknown sample. 3.+4. Group and selective reactions of anions, group reagents: BaCl2, AgNO3. Analysis of an unknown sample. 5.+6. Elemental analysis, confirmation of important functional groups: alcohol, aldehydes, carboxylic acids, amines. Preliminary test, determination of the solubility class. Analysis of unknown samples. 7.+8. Refractive index measurement, determination of melting point. pH measurement - determination of a weak acid 9.+10. UV-VIS qualitative analysis of organic compounds. Analysis of an unknown sample from a UV-VIS spectrum. Spectrum of an acid-base indicator in acidic and basic pH. 11.+12. IR qualitative analysis of organic compounds. Transmission and reflection modes (ATR). Analysis of an unknown sample.

Studijní zdroje a literatura

povinná literatura
• Skoog, West. Fundamentals of Analytical Chemistry. URL, URL info

doporučená literatura
• European Pharmacopoeia. URL, URL info

Přístupy, postupy a metody používané ve výuce

Monologic (reading, lessons, demonstration) Laboratory work

Způsob ověření výstupů z učení a požadavky na ukončení

To get credits a student must: -take part in all the laboratory exercises -submit protols from all the laboratory exercises -51% of correct answers of a final credit test

Vyučovací jazyk

Angličtina

Odkaz a informace vyučujících

https://moodlinka.ics.muni.cz

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Nachází se v prerekvizitách jiných předmětů

• FAAI2_15 Analytical Chemistry II
  FAAI1_15 && studijni_skupina(start_before_2025) || program(KOS)  

• Statistika zápisu (nejnovější)
  
• Permalink: https://is.muni.cz/predmet/pharm/podzim2025/FAAI1_15