Lab ID Naftalen Biphenyl Acenaftylen Acenaften Fluoren Fenantren Antracen Fluoranten Pyren Reten Benzo(b)fluorene Benzo-Naphtho-Thiophene Benzo(ghi)fluoranthene Cyclopenta(cd)pyrene Benz(a)antracen Triphenylene Chrysen Benzo(b)fluoranten Benzo(j)fluoranthene Benzo(k)fluoranten Benzo(e)pyrene Benzo(a)pyren Perylene Indeno(123cd)pyren Dibenz(ah)antracen Dibenzo(ac)anthracene Benzo(ghi)perylen Anthanthrene Coronene SUM 16 PAH SUM 29 PAH D8-Naftalen D10-Fenantren D12-Perylen Compound LOQ ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek ng/vzorek 16 PAHs Naftalen 0.074 K_A 430.540 162.928 11.460 56.125 174.174 431.443 21.100 149.895 87.119 53.858 8.032 0.553 7.302 5.190 2.627 9.965 4.039 1.637 1.808 2.349 2.128 0.382 2.072 0.216 0.193 2.304 0.248 0.902 1389.58 1630.59 240.62 263.48 287.63 Acenaftylen 0.102 L_C_H 353.725 200.639 7.220 72.441 301.268 954.183 43.105 396.327 260.705 97.743 21.140 2.448 22.108 19.227 7.452 31.397 17.866 8.171 8.500 11.663 11.915 2.182 10.783 1.072 0.984 12.734 1.481 4.235 2502.47 2882.72 203.68 247.10 237.89 Acenaften 0.089 M_H_K 433.781 261.148 35.412 58.369 48.784 378.780 7.656 40.271 12.208 12.260 0.548 0.242 0.999 0.289 0.450 0.719 1.076 0.720 0.269 0.229 0.584 0.274 0.354 0.802 0.270 1019.17 1296.50 249.55 246.43 267.08 Fluoren 0.100 S_K_S 280.757 153.684 3.434 41.900 185.787 447.846 7.118 129.620 60.227 33.877 5.310 0.561 5.071 3.036 2.593 8.102 3.580 1.826 1.606 2.184 1.822 0.306 1.767 0.216 0.156 1.891 0.196 0.591 1178.71 1385.06 264.56 311.33 271.25 Fenantren 0.072 SM 399.179 167.990 11.460 57.678 178.294 500.934 23.821 145.343 85.180 43.340 7.497 0.525 7.059 5.096 2.319 10.022 4.172 1.602 1.832 2.426 2.340 0.396 2.164 0.249 0.214 2.396 0.296 0.846 1430.16 1664.67 257.79 315.28 288.32 Antracen 0.100 SO 791.053 294.889 92.718 68.573 307.471 1109.632 137.846 456.593 319.390 32.038 24.976 1.279 23.082 19.364 5.754 26.575 10.570 4.428 5.015 6.441 8.280 1.448 6.169 0.603 0.622 6.205 1.044 1.901 3366.06 3763.96 184.06 225.16 260.91 Fluoranten 0.028 LP1 590.708 445.637 33.032 121.237 790.129 3759.786 445.869 1703.096 1270.432 89.644 125.338 0.874 76.357 58.320 13.692 72.109 20.392 10.179 9.583 12.139 10.359 1.490 12.270 0.923 0.784 12.621 0.518 4.209 8910.87 9691.73 209.60 274.61 269.24 Pyren 0.029 B4 1547.163 1021.314 174.885 413.886 1512.715 9601.488 1475.797 3529.619 2496.011 542.052 265.834 4.394 150.674 148.640 34.827 174.749 88.519 53.306 42.914 53.047 40.923 6.842 62.420 5.014 4.403 57.634 2.914 20.684 21372.38 23532.67 204.99 290.68 279.01 Benz(a)antracen 0.023 RP6 613.259 403.626 35.824 132.115 798.522 3124.213 331.370 1340.042 917.821 353.645 103.082 2.007 59.715 48.521 11.904 62.371 20.340 10.963 10.124 11.603 11.085 1.723 13.133 1.040 0.994 12.464 0.688 4.376 7472.24 8436.57 203.48 287.10 289.67 Chrysen 0.019 KK4 192.270 148.883 9.876 62.326 394.892 1875.672 183.835 988.164 668.379 281.625 76.093 10.922 47.799 87.067 19.707 92.619 73.918 34.991 38.208 53.223 68.571 13.833 60.572 7.049 6.160 59.472 10.843 18.335 4862.89 5585.30 106.00 229.83 252.49 Benzo(b)fluoranten 0.086 SHuf 355.221 235.599 34.342 83.345 466.878 1652.670 189.053 804.515 541.082 124.811 56.617 2.336 39.552 34.267 8.532 44.534 19.316 7.677 8.899 11.390 11.876 2.023 12.059 1.159 1.159 11.832 1.285 4.032 4271.05 4766.07 115.09 212.34 278.87 Benzo(k)fluoranten 0.096 KD 459.893 148.922 15.704 50.954 179.886 503.947 20.957 185.576 107.957 86.953 9.660 1.075 9.245 8.394 3.268 13.995 7.963 3.361 3.486 4.823 5.374 0.993 4.851 0.532 0.479 5.249 0.867 1.918 1574.72 1846.28 190.58 250.78 306.31 Benzo(a)pyren 0.119 KS 182.403 370.853 31.132 135.662 806.571 3136.869 438.457 1402.881 1016.583 198.087 112.215 6.532 63.747 72.664 14.982 81.592 40.820 17.552 19.822 26.607 32.913 5.921 28.449 3.069 2.788 29.041 4.863 10.786 7458.93 8293.86 44.44 262.17 267.64 Indeno(123cd)pyren 0.076 PK_1 549.890 304.344 33.720 116.753 549.300 1529.269 167.296 807.580 542.181 156.732 58.734 1.703 39.906 31.983 7.901 43.375 12.891 6.942 6.355 7.471 7.444 1.186 8.026 0.735 0.628 7.907 0.628 2.885 4414.71 5003.77 226.48 224.07 305.71 Dibenz(ah)antracen 0.058 SV2 307.948 222.349 19.257 54.619 366.071 1479.830 86.847 722.169 452.051 89.654 44.758 1.875 40.371 27.552 11.772 49.832 16.437 8.316 7.450 9.373 6.666 1.099 9.320 0.682 0.657 9.327 0.537 3.656 3616.06 4050.47 250.95 309.03 306.07 Benzo(ghi)perylen 0.062 GH 638.876 318.738 16.306 87.504 518.640 1972.413 181.234 1026.111 685.016 133.753 66.543 1.346 47.124 38.543 12.132 52.417 17.192 8.236 7.763 10.209 8.566 1.451 10.170 0.842 0.824 10.091 0.922 3.460 5271.68 5876.42 189.96 196.91 274.77 29 PAHs Biphenyl 0.043 SV1 561.595 269.760 9.785 136.419 449.836 1354.076 48.459 525.996 295.529 76.483 32.048 2.837 23.442 22.238 8.253 35.625 19.675 7.259 8.890 11.861 12.234 2.373 12.224 1.275 1.275 12.361 2.161 4.299 3506.21 3948.27 218.03 287.66 314.89 Reten 0.055 TS 901.173 430.780 34.622 899.459 332.338 1278.005 24.605 75.915 25.366 11.440 1.574 0.328 1.443 1.778 1.386 1.314 2.524 1.344 0.649 0.610 0.784 0.858 0.172 0.727 0.687 0.241 3579.62 4030.12 131.87 189.89 308.33 Benzo(b)fluorene 0.069 MZ 449.001 253.638 19.654 77.145 204.161 1387.932 78.323 566.936 338.428 97.539 32.545 2.356 29.415 23.413 9.536 38.908 16.519 6.431 6.981 9.264 7.830 1.297 8.816 0.768 0.784 8.786 0.823 3.212 3233.60 3680.44 259.81 344.75 346.51 Benzo-Naphtho-Thiophene 0.033 SH 239.712 148.774 64.798 66.067 90.341 286.475 15.714 29.060 21.496 7.184 0.982 0.188 1.066 1.299 0.871 0.819 1.542 0.749 0.490 0.399 0.505 0.484 0.136 0.402 0.406 0.125 818.52 980.08 251.91 273.90 282.21 Benzo(ghi)fluoranthene 0.023 MN 259.487 158.815 8.704 35.312 280.803 1010.570 19.067 422.619 231.189 84.335 21.565 1.666 19.040 12.287 6.299 27.447 10.835 4.502 4.886 5.863 4.613 0.885 5.632 0.583 0.442 5.494 0.470 1.923 2339.52 2645.33 216.88 278.56 310.28 Cyclopenta(cd)pyrene 0.054 MS-5 298.847 191.016 57.972 115.787 203.332 262.318 13.980 41.135 29.179 11.839 1.189 0.216 2.127 0.874 1.136 0.743 2.062 1.231 0.572 0.476 0.936 0.742 0.117 0.633 1.004 0.300 1029.84 1239.77 238.54 210.58 291.48 Triphenylene 0.017 PK_2 921.795 631.366 67.193 208.338 291.924 1026.633 26.383 136.532 50.397 15.493 1.934 0.462 3.607 0.483 1.814 1.546 3.231 1.915 0.713 0.740 1.463 1.288 0.221 1.099 0.093 0.099 2.034 0.208 0.607 2741.41 3399.61 260.24 222.61 313.29 Benzo(j)fluoranthene 0.091 VV 289.005 221.235 37.196 86.674 451.290 1328.699 192.060 664.103 449.489 191.536 60.101 1.753 34.004 31.656 7.112 40.069 14.587 6.476 7.100 8.545 9.479 1.572 9.528 0.891 0.811 8.771 1.001 2.988 3620.60 4157.73 133.41 223.11 295.02 Benzo(e)pyrene 0.079 NS 107.278 139.743 4.699 41.093 298.323 892.867 51.630 547.017 302.703 100.361 36.877 2.970 22.805 19.881 8.820 31.495 17.267 6.982 7.403 9.828 8.333 1.452 10.260 0.992 0.945 10.101 0.927 3.597 2351.34 2686.65 69.81 209.87 311.80 Perylene 0.091 Ir 313.831 173.646 34.750 100.722 132.864 367.605 17.383 39.643 21.812 14.859 1.183 0.209 1.326 0.642 0.835 0.907 1.684 1.278 0.559 0.441 0.709 0.517 0.084 0.479 0.639 0.189 1034.49 1228.80 167.74 196.48 301.90 Dibenzo(ac)anthracene 0.058 AB 305.353 177.055 9.334 96.922 305.327 841.474 34.582 440.189 269.327 140.867 24.604 1.436 22.901 13.786 5.563 28.625 8.993 4.729 4.278 5.577 4.607 0.834 5.004 0.508 0.460 5.797 0.587 1.995 2374.11 2760.72 212.73 254.47 322.54 Anthanthrene 0.119 Hanka 338.030 199.103 7.606 64.127 234.753 454.773 15.986 205.761 115.034 52.494 10.060 0.903 9.642 6.962 3.538 13.921 6.362 2.474 2.764 3.673 3.452 0.625 3.579 0.368 0.351 3.759 0.467 1.383 1477.24 1761.95 257.08 273.83 346.38 Coronene 0.096 AI 425.016 195.806 12.607 72.937 274.654 592.691 42.613 377.034 227.062 97.176 20.492 1.246 16.306 12.856 5.352 21.217 7.929 3.186 3.320 4.520 3.972 0.677 4.198 0.336 0.358 4.404 0.390 1.424 2082.85 2429.78 246.10 212.34 307.29 2KL 4.717 11.106 1.439 6.431 38.064 187.856 13.909 97.020 68.044 4.943 5.582 0.136 4.164 3.618 1.010 4.770 1.263 0.738 0.600 0.767 0.757 0.114 0.728 0.063 0.733 0.213 429.95 458.78 1.21 14.31 21.40 1MSL 356.604 243.663 23.731 54.197 296.807 825.211 72.191 350.347 223.946 83.543 23.085 0.922 17.779 14.502 5.754 22.666 8.741 4.649 4.102 5.470 4.848 0.712 5.217 0.443 0.439 5.583 0.460 1.941 2269.14 2657.55 218.92 214.41 274.58 3VK 311.994 312.899 36.413 513.226 618.218 1884.081 34.579 57.120 33.808 34.637 1.161 0.745 1.721 0.364 0.701 1.392 1.874 0.402 0.336 0.308 0.689 0.310 0.453 0.924 0.275 3494.41 3848.63 216.28 279.92 295.96 Pro výpočet % výtěžnosti metody (ztrát při přípravě) je potřeba porovnat množství D-PAHs s teoretickou 100% přidanou hodnotou (333 ng/vzorek) Prázdné buňky mají množství pod limitem kvantifikace (