C5241 Organic Analysis

Faculty of Science
Autumn 2013
Extent and Intensity
1/0/0. 1 credit(s) (plus extra credits for completion). Recommended Type of Completion: zk (examination). Other types of completion: k (colloquium).
Teacher(s)
RNDr. Marta Farková, CSc. (lecturer)
prof. RNDr. Přemysl Lubal, Ph.D. (lecturer)
doc. RNDr. Pavel Pazdera, CSc. (lecturer)
Guaranteed by
RNDr. Marta Farková, CSc.
Department of Chemistry - Chemistry Section - Faculty of Science
Supplier department: Department of Chemistry - Chemistry Section - Faculty of Science
Timetable
Wed 13:00–14:50 C14/207
Prerequisites
C2021 - Organic chemistry I C3100 + C4050 Analytical chemistry (at least C1660)
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
Course objectives
The aim of the course is to inform students about classical organic analysis = characteristic physical properties of organic compounds, elemental analysis of organic compounds, analytical identification and determination of important functional groups of organic compounds, mainly by colour reactions in solution. Interpretation of spectra of simple organic compounds obtained by instrumental methods: UV-VIS, IR, NMR, MS.
Syllabus
  • Characteristics of organic compounds analysis. The methodology of the analysis, development and trends. Determination of physical constants: melting and boiling point, refractivity, optical activity, partition coefficients of extraction, molecular weight, spectral constants. Determination of purity, purification of sample. Elemental analysis. Sample decomposition, detection and determination of C, H, O, N, Cl, Br, I, S, P, F. Automatic methods of elemental analysis. Functional groups identification: classes of dissolution, classification reactions for carbohydrates, alcohols, phenols, aldehydes, ketones, carboxylic acids, acid anhydrides, esters, amides, imides, ethers, epoxides, peroxides, amines, hydroxylamines, nitriles, isocyanides, nitro-, nitroso-, azo-, azoxy-, hydrazo- and diazocompounds, thiols, sulphonic and sulphinic acids and their derivatives, halogen compounds. Methods and procedures for identification of organic compounds. Determination of organic compounds based on their functional groups reactions (acid-base and redox reaction; determination of gases; determination of reaction water; gravimetry of insoluble compounds; spectrophotometry; electroactivity - coulometry, polarography and similar methods; separations).
Literature
  • STRÁNSKÝ, Zdeněk. Analýza organických sloučenin a. 1. vyd. Olomouc: Univerzita Palackého, 1981. 235 s. info
  • STRÁNSKÝ, Zdeněk. Analýza organických sloučenin b. 1. vyd. Olomouc: Univerzita Palackého, 1981. 235 s. info
  • KALOUS, Vítěz. Jak moderní chemie zkoumá strukturu molekul. 1. vyd. Praha: SNTL - Nakladatelství technické literatury, 1983. 150 s. info
  • HOLZBECHER, Záviš. Analytická chemie [Holzbecher, 1974]. 2. přeprac. vyd. Praha: SNTL - Nakladatelství technické literatury, 1974. 506 s. info
  • STUŽKA, Václav. Instrumentální metody chemické analysy. I, Elektronová spektroskopie organických molekul. 1. vyd. Olomouc: Univerzita Palackého, 1974. 111 s. info
  • STUŽKA, Václav. Instrumentální metody chemické analysy. II, Hmotová spektroskopie organických molekul. 1. vyd. Olomouc: Univerzita Palackého, 1975. 128 s. info
  • STUŽKA, Václav. Instrumentální metody chemické analýzy. IV, Vibrační spektroskopie organ. molekul. 1. vyd. Olomouc: Univerzita Palackého, 1976. 146 s. info
Teaching methods
Type of education: lectures, class discussion
Assessment methods
Type of exam: written and oral exam. Exam consists of basic questions, which are expanded during the examination to allow the student to demonstrate the extent of topic understanding.
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
Study Materials
The course can also be completed outside the examination period.
The course is taught annually.
Listed among pre-requisites of other courses
Teacher's information
http://www.chemi.muni.cz/~pazourek/
The course is also listed under the following terms Autumn 2007 - for the purpose of the accreditation, Autumn 1999, Autumn 2010 - only for the accreditation, Autumn 2000, Autumn 2001, Autumn 2002, Autumn 2003, Autumn 2004, Autumn 2005, Autumn 2006, Autumn 2007, Autumn 2008, Autumn 2009, Autumn 2010, Autumn 2011, Autumn 2011 - acreditation, Autumn 2012, Autumn 2014, Autumn 2015, Autumn 2016, autumn 2017, Autumn 2018, Autumn 2019, Autumn 2020.
  • Enrolment Statistics (Autumn 2013, recent)
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