PřF:C6860 Modern Meth. Pollutant Anal. - Course Information
C6860 Modern Methods of Pollutant AnalysisFaculty of Science
- Extent and Intensity
- 2/0/0. 2 credit(s) (plus extra credits for completion). Recommended Type of Completion: zk (examination). Other types of completion: k (colloquium).
- prof. RNDr. Jana Klánová, Ph.D. (lecturer)
prof. RNDr. Josef Komárek, DrSc. (lecturer)
prof. RNDr. Jakub Hofman, Ph.D. (assistant)
- Guaranteed by
- RECETOX - Faculty of Science
- C6110 course, Environmental Analytical Chemistry or an equivalent should be passed.
- Course Enrolment Limitations
- The course is also offered to the students of the fields other than those the course is directly associated with.
- fields of study / plans the course is directly associated with
- there are 23 fields of study the course is directly associated with, display
- Course objectives
- Aim of the course is an enhancement of knowledges acquired in course C6110, Environmental Analytical Chemistry. Part engaged in organic contaminants (A. Hrdlička) deals mainly with contemporary techniques of sample preparation and with techniques hyphenating high performance separation with specific detection. Treatment of environmental samples with various matrices is discussed. In the part on inorganic contaminants (J. Komárek) requirements for trace inorganic analysis are introduced and, further, flow injection analysis, speciation of elements by electrochemical methods and by gas chromatography, applications of liquid chromatography and other techniques are discussed.
- Part A: ORGANIC POLLUTANTS (by A. Hrdlička) A.I. Specific problems of organic pollutants analysis. A.II. Contemporary techniques of sample preparation. Automatized Soxhlet extraction, MAE, ASE, SFE, SPE, SPME, molecular imprints. Cloud-point extraction and polymer mediated extraction. Headspace, purge&trap. Membrane separations. Recovery estimation. A.III. Preparation of water, sediment, soil, and biota samples. Automation, on-line techniques. Multiresidual schema. Direct methods. A.IV. Hyphenated techniques: GC/FTIR, LC/FTIR, GC/OES, GC/AED, HPLC/NMR. Part B: INORGANIC POLLUTANTS (by J. Komárek) B.I. Trace inorganic analysis, practical aspects. B.II. Flow analysis, instrumentation, preconcentration. B.III. Electrochemical techniques for element speciation, ASV, electrodeposition, electrodes. B.IV. Speciation of elements by GC. Derivatization, termic desorption, detection means. Sample preparation. B.V. HPLC application, ion chromatography, GPC. Detection means. B.VI. Other techniques, LIDAR.
- BARCELÓ, D. Environmental Analysis. Techniques, Applications and Quality Assurance. Amsterdam: Elsevier, 1993. Techniques & Instrumentation Anal. Chem., Vol. 13. ISBN 0-444-89648-1. info
- BUFFINGTON, R. GC-Atomic Emission Spectroscopy Using Microwave Plasmas. Avandale, USA: Hewlett-Packard, 1988. ISBN 05921-90100. info
- KALOUS, Vítěz. Metody chemického výzkumu. 1. vyd. Praha: SNTL - Nakladatelství technické literatury, 1987. 430 s. info
- LOPEZ-AVILA, V. Sample Preparation for Environmental Analysis. Critical Reviews in Analytical Chemistry, 1999, vol. 29, No 3, p. 195-230. ISSN 1040-8347. info
- Assessment methods (in Czech)
- přednášky, ústní zkouška
- Language of instruction
- Further comments (probably available only in Czech)
- The course is taught annually.
The course is taught: every week.
General note: Navazuje na předmět C6110 Anal. chemie živ. prostředí.