Simultaneous System of DP-LIBS and Laser Ablation ICP-OES

NOVOTNÝ, Karel, Aleš HRDLIČKA, Kateřina ŠTĚPÁNKOVÁ, Viktor KANICKÝ, Jozef KAISER, Radomír MALINA and David HAHN. Simultaneous System of DP-LIBS and Laser Ablation ICP-OES. In ESAS 2012. 2012. ISBN 978-80-223-3292-7.

Basic information

• Original name: Simultaneous System of DP-LIBS and Laser Ablation ICP-OES
• Name in Czech: Simultánní systém DP-LIBS a Laserová ablace ve spojení s ICP-OES
• Authors: NOVOTNÝ, Karel (203 Czech Republic, guarantor, belonging to the institution), Aleš HRDLIČKA (203 Czech Republic, belonging to the institution), Kateřina ŠTĚPÁNKOVÁ (203 Czech Republic, belonging to the institution), Viktor KANICKÝ (203 Czech Republic, belonging to the institution), Jozef KAISER (203 Czech Republic), Radomír MALINA (203 Czech Republic) and David HAHN (840 United States of America).
• Edition: ESAS 2012, 2012.

Other information

• Original language: English
• Type of outcome: Conference abstract
• Field of Study: 10406 Analytical chemistry
• Country of publisher: Slovakia
• Confidentiality degree: is not subject to a state or trade secret
• WWW: URL
• RIV identification code: RIV/00216224:14740/12:00061416
• Organization unit: Central European Institute of Technology
• ISBN: 978-80-223-3292-7
• Keywords (in Czech): LIBS; Laserová ablace; ICP-OES
• Keywords in English: LIBS; Laser ablation; ICP-OES
• Tags: International impact

Abstract

The simultaneous DP-LIBS and Laser-Ablation ICP-OES setup was designed by utilizing a modified commercially available laser ablation system UP-266 Macro (New Wave). Specially designed ablation chamber was developed to allow combination LIBS, DP-LIBS and LA-ICP-OES technique. In preliminary results washout efficiency of new ablation chamber was verified. Basic signal comparison of DP-LIBS and double pulse LA-ICP-OES were studied on the urinary stone cross-section. Results demonstrate high sensitivity for both methods and high spatial resolution.

Abstract (in Czech)

Simultánní systém DP-LIBS a Laserové ablace ve spojení s ICP-OES spektrometrií byl navržen s využitím modifikovaného komerčního systému UP-266 Macro (New Wave). Speciálně vyvinutá ablační komora byla konstruována pro možnost kombinace technik LIBS, DP-LIBS a LA-ICP-OES spektrometrie. V předběžných experimentech byla ověřena vysoká efektivita průplachu komory. Základní porovnání signálů DP-LIBS a LA-ICP-OES technik bylo provedeno na řezu močového kamene. Výsledky ukazují vysokou citlivost obou metod a vysoké prostorové rozlišení.

Links

• ED1.1.00/02.0068, research and development project: Name: CEITEC - central european institute of technology
• ME08002, research and development project: Name: Použití spektroskopie laserem buzeného plazmatu (LIBS) a laserové ablace ve spojení s ICP-OES/MS spektroskopií pro chemické mapování biominerálů

Investor: Ministry of Education, Youth and Sports of the CR, Utilization of the laser induced breakdown spectroscopy (LIBS) and laser ablation ICP-OES/MS spectroscopy for chemical mapping of biominerals, Research and Development Programme KONTAKT (ME)