DAVID, Bohumil, Oldřich SCHNEEWEISS, Naděžda PIZÚROVÁ, Antonín REK, Vít KUDRLE a Ondřej JAŠEK. NANOSTRUCTURED ALPHA-FE LAYERS SYNTHESIZED IN LOW-PRESSURE MICROWAVE PLASMA. In Nanocon 2012. 2012. ISBN 978-80-87294-35-2.
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Základní údaje
Originální název NANOSTRUCTURED ALPHA-FE LAYERS SYNTHESIZED IN LOW-PRESSURE MICROWAVE PLASMA
Autoři DAVID, Bohumil, Oldřich SCHNEEWEISS, Naděžda PIZÚROVÁ, Antonín REK, Vít KUDRLE a Ondřej JAŠEK.
Vydání Nanocon 2012, 2012.
Další údaje
Originální jazyk angličtina
Typ výsledku Konferenční abstrakt
Obor 10305 Fluids and plasma physics
Stát vydavatele Česká republika
Utajení není předmětem státního či obchodního tajemství
Organizační jednotka Přírodovědecká fakulta
ISBN 978-80-87294-35-2
Klíčová slova anglicky nanomaterial; plasma synthesis; iron layer
Změnil Změnil: prof. Mgr. Vít Kudrle, Ph.D., učo 2560. Změněno: 11. 7. 2015 15:07.
Anotace
We have used microwave plasma at the low pressure of 2 kPa to synthesize nanostructured alpha-Fe layer. This layer was deposited on a glass substrate which was immersed in Ar plasma (microwave power of 250 W). Iron pentacarbonyl Fe(CO)5 was flown over the substrate and its decomposition resulted in the formation of a few micrometers thick fully nanostructured iron layer. The deposition time was 60 seconds. The synthesized samples were studied using XRD, SEM, EDAX and 57Fe Mossbauer spectrometry. Only alpha-Fe phase with the mean crystallite size of 14 nm was observed in the XRD pattern of the representative sample. It was observed in SEM that the fine structure of the layer exhibited a kind of columnar structure whereby the columns were formed of nanocrystals. No voids were observed and oxygen, due to its low concentration, was hardly detectable with EDAX. In the transmission Mossbauer spectrum, as well as in the conversion-electron Mossbauer spectrum, collected on the pieces of the layer, alpha-Fe sextet dominated and a surprisingly low amount of iron oxides was identified (respective spectrum area was about 1 %). It means that the pieces of alpha-Fe layer were very weakly oxidized.
VytisknoutZobrazeno: 1. 12. 2022 10:36