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@article{1371252,
author = {Hassan, Walid Fathalla M. and Ali, Ibrahim A. I. and Pazdera, Pavel},
article_number = {June},
doi = {http://dx.doi.org/10.3762/bjoc.13.20},
keywords = {heterocyclic amides; heterocyclic thioamides; N-cyclohexyl dithiocarbamate cyclohexylammonium salt; novel thiating agent; thiation},
language = {eng},
issn = {1860-5397},
journal = {Beilstein Journal of Organic Chemistry},
title = {A novel method for heterocyclic amide–thioamide transformations},
url = {https://www.beilstein-journals.org/bjoc/content/pdf/1860-5397-13-20.pdf},
volume = {13},
year = {2017}
}
TY - JOUR
ID - 1371252
AU - Hassan, Walid Fathalla M. - Ali, Ibrahim A. I. - Pazdera, Pavel
PY - 2017
TI - A novel method for heterocyclic amide–thioamide transformations
JF - Beilstein Journal of Organic Chemistry
VL - 13
IS - June
SP - 174-181
EP - 174-181
SN - 18605397
KW - heterocyclic amides
KW - heterocyclic thioamides
KW - N-cyclohexyl dithiocarbamate cyclohexylammonium salt
KW - novel thiating agent
KW - thiation
UR - https://www.beilstein-journals.org/bjoc/content/pdf/1860-5397-13-20.pdf
L2 - https://www.beilstein-journals.org/bjoc/content/pdf/1860-5397-13-20.pdf
N2 - In this paper, we introduce a novel and convenient method for the transformation of heterocyclic amides into heteocyclic thioamides. A two-step approach was applied for this transformation: Firstly, we applied a chlorination of the heterocyclic amides to afford the corresponding chloroheterocycles. Secondly, the chloroherocycles and N-cyclohexyl dithiocarbamate cyclohexylammonium salt were heated in chloroform for 12 h at 61 °C to afford heteocyclic thioamides in excellent yields.
ER -
HASSAN, Walid Fathalla M., Ibrahim A. I. ALI a Pavel PAZDERA. A novel method for heterocyclic amide–thioamide transformations. \textit{Beilstein Journal of Organic Chemistry}. roč.~13, June, s.~174-181. ISSN~1860-5397. doi:10.3762/bjoc.13.20. 2017.
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