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@proceedings{1394328,
author = {Borůvka, Tomáš and Vykoukal, Vít and Zelenka, František and Pinkas, Jiří},
booktitle = {NANOCON 2017},
keywords = {Nanoparticles; Tin; Melting point depression; reduction synthesis; DLS; DSC; TEM; SEM; PXRD},
language = {eng},
title = {Preparation and characterization of tin nanoparticles},
year = {2017}
}
TY - CONF
ID - 1394328
AU - Borůvka, Tomáš - Vykoukal, Vít - Zelenka, František - Pinkas, Jiří
PY - 2017
TI - Preparation and characterization of tin nanoparticles
KW - Nanoparticles
KW - Tin
KW - Melting point depression
KW - reduction synthesis
KW - DLS
KW - DSC
KW - TEM
KW - SEM
KW - PXRD
N2 - In this work we study preparation methods of tin nanoparticles in different reaction conditions, then we study influence of reaction temperature, surfactant type and amount on size and melting point of nanoparticles. Prepared nanoparticles are characterized by dynamic light scattering, transmission and scanning electron microscopy, differential scanning calorimetry and powder X-ray diffraction. Results of individual analyses are mutually compared and the process of preparing the nanoparticles exhibiting the highest uniformity, depression of melting point and the lowest size evaluated. The smallest particles were synthetised by the reduction method at temperature of 120 °C and their diameter was 10 nm. Melting point depression of this sample is reported, it melte dat 225 °C.
ER -
BORŮVKA, Tomáš, Vít VYKOUKAL, František ZELENKA and Jiří PINKAS. Preparation and characterization of tin nanoparticles. In \textit{NANOCON 2017}. 2017.
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