Detailed Information on Publication Record
2017
Preparation and characterization of tin nanoparticles
BORŮVKA, Tomáš, Vít VYKOUKAL, František ZELENKA and Jiří PINKASBasic information
Original name
Preparation and characterization of tin nanoparticles
Name in Czech
Příprava a charakterizace nanočástic cínu
Authors
BORŮVKA, Tomáš (203 Czech Republic, belonging to the institution), Vít VYKOUKAL (203 Czech Republic, belonging to the institution), František ZELENKA (203 Czech Republic, belonging to the institution) and Jiří PINKAS (203 Czech Republic, guarantor, belonging to the institution)
Edition
NANOCON 2017, 2017
Other information
Language
English
Type of outcome
Konferenční abstrakt
Field of Study
10402 Inorganic and nuclear chemistry
Country of publisher
Czech Republic
Confidentiality degree
není předmětem státního či obchodního tajemství
RIV identification code
RIV/00216224:14310/17:00095135
Organization unit
Faculty of Science
Keywords (in Czech)
Nanočástice; cin; pokles teploty tání; redukční syntéza; DLS; DSC; TEM; SEM; PXRD
Keywords in English
Nanoparticles; Tin; Melting point depression; reduction synthesis; DLS; DSC; TEM; SEM; PXRD
Tags
International impact, Reviewed
Změněno: 8/10/2018 15:29, prof. RNDr. Jiří Pinkas, Ph.D.
Abstract
V originále
In this work we study preparation methods of tin nanoparticles in different reaction conditions, then we study influence of reaction temperature, surfactant type and amount on size and melting point of nanoparticles. Prepared nanoparticles are characterized by dynamic light scattering, transmission and scanning electron microscopy, differential scanning calorimetry and powder X-ray diffraction. Results of individual analyses are mutually compared and the process of preparing the nanoparticles exhibiting the highest uniformity, depression of melting point and the lowest size evaluated. The smallest particles were synthetised by the reduction method at temperature of 120 °C and their diameter was 10 nm. Melting point depression of this sample is reported, it melte dat 225 °C.
Links
| GA17-15405S, research and development project |
| ||
| LM2015043, research and development project |
| ||
| LQ1601, research and development project |
|