GABLECH, I., Ondřej CAHA, V. SVATOŠ, J. PRÁŠEK, J. PEKÁREK, P. NEUŽIL and Tomáš ŠIKOLA. PREPARATION OF [001] ORIENTED TITANIUM THIN FILM FOR MEMS APPLICATIONS BY KAUFMAN ION-BEAM SOURCE. In 9TH INTERNATIONAL CONFERENCE ON NANOMATERIALS - RESEARCH & APPLICATION (NANOCON 2017). SLEZSKA: TANGER LTD, 2018, p. 117-122. ISBN 978-80-87294-81-9.
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Basic information
Original name PREPARATION OF [001] ORIENTED TITANIUM THIN FILM FOR MEMS APPLICATIONS BY KAUFMAN ION-BEAM SOURCE
Authors GABLECH, I., Ondřej CAHA (203 Czech Republic, guarantor, belonging to the institution), V. SVATOŠ, J. PRÁŠEK, J. PEKÁREK, P. NEUŽIL and Tomáš ŠIKOLA (203 Czech Republic).
Edition SLEZSKA, 9TH INTERNATIONAL CONFERENCE ON NANOMATERIALS - RESEARCH & APPLICATION (NANOCON 2017), p. 117-122, 6 pp. 2018.
Publisher TANGER LTD
Other information
Original language English
Type of outcome Proceedings paper
Field of Study 10302 Condensed matter physics
Confidentiality degree is not subject to a state or trade secret
Publication form printed version "print"
RIV identification code RIV/00216224:14310/18:00106417
Organization unit Faculty of Science
ISBN 978-80-87294-81-9
UT WoS 000452823300018
Keywords in English Titanium thin film; [001] orientation; stress-free; thermal coefficient of resistivity; resistivity
Tags International impact, Reviewed
Changed by Changed by: doc. Mgr. Ondřej Caha, Ph.D., učo 4414. Changed: 1/3/2019 11:29.
Abstract
We propose the sputtering deposition providing titanium thin films with controlled properties such as preferential crystallography and residual stress using Kaufman ion-beam source. The titanium thin films with thickness of approximate to 80 nm were deposited on [001] Si wafer covered by SiO2 deposited by plasma-enhanced chemical vapor deposition. To achieve the required crystallography and stress properties, we investigated the different beam voltage of Kaufman ion-beam source and controlled the substrate temperature during deposition using a built-in heater. We used two X-ray diffraction methods to determine the planes parallel to the sample surface and residual stress. We also measured the current-voltage curves to determine the resistivity (rho) and the thermal coefficient of resistivity (alpha) of titanium thin films at different substrate temperatures using 4-probe measurement setup. We showed that it is possible to prepare stress-free titanium thin films with pure [001] orientation at the lowest beam voltage of 200 V and substrate temperature of approximate to 273 degrees C. The corresponding lattice parameters a(0) and c(0) were (2.954 +/- 0.003) angstrom and (4.695 +/- 0.001) angstrom, respectively. Electrical parameters of this sample as rho and alpha were (9.2 +/- 0.1).10(-7) Omega.m and (2.6 +/- 0.2).10(-3) K-1, respectively. We found out that these layers are well suitable for micro-electro-mechanical systems where the pure [001] orientation, no residual stress and low rho and high alpha are essential. We found that rho and a are dependent on each other. The rho value was approximate to 2x higher than the bulk material value, which is an excellent result for a thin film with the thickness of approximate to 80 nm.
Links
LM2015041, research and development projectName: CEITEC Nano
Investor: Ministry of Education, Youth and Sports of the CR
LO1411, research and development projectName: Rozvoj centra pro nízkonákladové plazmové a nanotechnologické povrchové úpravy (Acronym: CEPLANT plus)
Investor: Ministry of Education, Youth and Sports of the CR
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