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@article{1832377,
author = {Březina, Adam and Dořmanová, Adéla and Kukučka, Petr and Lubal, Přemysl and Farková, Marta},
article_location = {Brno},
article_number = {5},
doi = {http://dx.doi.org/10.54779/ccsss20220319},
language = {cze},
issn = {2336-7202},
journal = {Czech Chemical Society Symposium Series},
title = {Aplikace transesterifikační derivatizační reakce pro GC-MS analýzy},
url = {https://doi.org/10.54779/ccsss20220319},
volume = {20},
year = {2022}
}
TY - JOUR
ID - 1832377
AU - Březina, Adam - Dořmanová, Adéla - Kukučka, Petr - Lubal, Přemysl - Farková, Marta
PY - 2022
TI - Aplikace transesterifikační derivatizační reakce pro GC-MS analýzy
JF - Czech Chemical Society Symposium Series
VL - 20
IS - 5
SP - 319-322
EP - 319-322
PB - Mendelova univerzita v Brně, Brno, Česká republika
SN - 23367202
UR - https://doi.org/10.54779/ccsss20220319
N2 - This paper is focused on study of the concentration of the basic catalyst in methanol on the yield of the derivatization transesterification reaction of triacyglycerols. Potassium hydroxide and sodium hydroxide solutions were used as basic catalysts. Triacylglycerols were transesterified, rapeseed oil was used as a sample. Triacylglycerols were converted to methyl esters of fatty acids, which were subsequently determined by GC-MS where the peak areas were monitored, because they represent the yield of the formed fatty acid methyl esters, namely palmitic, oleic, linoleic and stearic acids. The highest yield of transesterification of the oil to methylesters of fatty acids was found for a concentration of 3.0 mol dm–3 for KOH and 2.0 mol dm–3 for NaOH. At higher catalyst concentrations, a predominant side-reaction, saponification, was observed, which decreased the overall yield of fatty acid methyl esters.
ER -
BŘEZINA, Adam, Adéla DOŘMANOVÁ, Petr KUKUČKA, Přemysl LUBAL and Marta FARKOVÁ. Aplikace transesterifikační derivatizační reakce pro GC-MS analýzy. \textit{Czech Chemical Society Symposium Series}. Brno: Mendelova univerzita v Brně, Brno, Česká republika, 2022, vol.~20, No~5, p.~319-322. ISSN~2336-7202. Available from: https://dx.doi.org/10.54779/ccsss20220319.
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