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@article{197549, author = {Kanický, Viktor and Mermet, Jean and Michel}, article_location = {Berlin}, article_number = {7/8}, keywords = {Inductively Coupled Plasma; Atomic Emission Spectrometry; Laser Ablation; Silicates; Lithiumtetraborate Fusion;}, language = {eng}, issn = {0937-0633}, journal = {Fresenius Journal of Analytical Chemistry}, note = {Project PECO No. ERB3510PL921006}, title = {Selection of internal standards for analysis of silicate rocks and limestones by laser ablation inductively coupled plasma atomic emission spectrometry}, volume = {355}, year = {1996} }
TY - JOUR ID - 197549 AU - Kanický, Viktor - Mermet, Jean - Michel PY - 1996 TI - Selection of internal standards for analysis of silicate rocks and limestones by laser ablation inductively coupled plasma atomic emission spectrometry JF - Fresenius Journal of Analytical Chemistry VL - 355 IS - 7/8 SP - 887 EP - 887 PB - Springer-Verlag SN - 09370633 N1 - Project PECO No. ERB3510PL921006 KW - Inductively Coupled Plasma KW - Atomic Emission Spectrometry KW - Laser Ablation KW - Silicates KW - Lithiumtetraborate Fusion; N2 - Included (Si, Ca) and added (Li, B) internal standards (IS) have been used comparatively in LA-ICP AES of silicates and limestones to improve both precision and accuracy. A Q-switched Nd:YAG laser (355 nm, 10 Hz, 10 mJ per shot) has been applied for ablation, Samples have been prepared by fusion with Li2B4O7 and measured using a Perkin-Elmer Optima 3000 ICP system, Both types of IS have given a relative standard deviation (RSD) less than 2-1%, which improved the repeatability by a factor of 2-10 and calibration graphs have been linear over the whole concentration range. ER -
KANICKÝ, Viktor a Jean - Michel MERMET. Selection of internal standards for analysis of silicate rocks and limestones by laser ablation inductively coupled plasma atomic emission spectrometry. \textit{Fresenius Journal of Analytical Chemistry}. Berlin: Springer-Verlag, 1996, roč.~355, 7/8, s.~887-888. ISSN~0937-0633.
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