KANICKÝ, Viktor, Jan MUSIL and Jean - Michel MERMET. Determination of Zr and Ti in 3-micrometers-thick ZrTiN ceramic coatings using laser ablation inductively coupled plasma atomic emission spectrometry. Online. Applied Spectroscopy. USA: Society Appl. Spectroscopy, 1997, vol. 51, No 7, p. 1037-1041. ISSN 0003-7028. [citováno 2024-04-24]
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Basic information
Original name Determination of Zr and Ti in 3-micrometers-thick ZrTiN ceramic coatings using laser ablation inductively coupled plasma atomic emission spectrometry
Authors KANICKÝ, Viktor (203 Czech Republic, guarantor), Jan MUSIL (203 Czech Republic) and Jean - Michel MERMET (250 France)
Edition Applied Spectroscopy, USA, Society Appl. Spectroscopy, 1997, 0003-7028.
Other information
Original language English
Type of outcome Article in a journal
Field of Study 10406 Analytical chemistry
Country of publisher United States of America
Confidentiality degree is not subject to a state or trade secret
Impact factor Impact factor: 1.848
Organization unit Faculty of Science
Keywords in English Atomic emission spectrometry; inductively coupled plasma; UV laser ablation; Coating analysis; Nitride ceramic coatings
Tags atomic emission spectrometry, Coating analysis, inductively coupled plasma, Nitride ceramic coatings, UV laser ablation
Tags Reviewed
Changed by Changed by: prof. RNDr. Viktor Kanický, DrSc., učo 408. Changed: 29/6/2007 09:49.
Abstract
Analysis of 3-mu m-thick ZrN, TIN, and ZrTiN ceramic coatings on a high-speed steel substrate by laser ablation inductively coupled plasma atomic emission spectrometry (LA-ICP-AES) is described, A Nd:YAG laser was used in the Q-switched mode and operated at 355 nm and 5 mJ, Ablation patterns were obtained on the target surface by moving the ablation chamber with respect to the laser beam by means of an X-Y translator, Control of the depth of penetration was obtained by successively performing a limited number of cycles. Transient signals were obtained and their peak areas were used for the construction of calibration graphs based on the concentrations determined by energy-dispersive X-ray (EDX) analysis, An erosion rate of 0.1 mu m per cycle was observed, Crater shape and depth, temporal behavior, and reproducibility of the signals are described.
Abstract (in Czech)
Analysis of 3-mu m-thick ZrN, TIN, and ZrTiN ceramic coatings on a high-speed steel substrate by laser ablation inductively coupled plasma atomic emission spectrometry (LA-ICP-AES) is described, A Nd:YAG laser was used in the Q-switched mode and operated at 355 nm and 5 mJ, Ablation patterns were obtained on the target surface by moving the ablation chamber with respect to the laser beam by means of an X-Y translator, Control of the depth of penetration was obtained by successively performing a limited number of cycles. Transient signals were obtained and their peak areas were used for the construction of calibration graphs based on the concentrations determined by energy-dispersive X-ray (EDX) analysis, An erosion rate of 0.1 mu m per cycle was observed, Crater shape and depth, temporal behavior, and reproducibility of the signals are described.
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