MAREK, Radek, Pavlína SEČKÁŘOVÁ, Dagmar HULOVÁ, Jaromír MAREK, Jiří DOSTÁL and Vladimír SKLENÁŘ. Palmatine and Berberine Isolation Artifacts. Journal of Natural Products. American Chemical Society, vol. 66, No 4, p. 481-486. ISSN 1520-6025. doi:10.1021/np0204996. 2003.
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Basic information
Original name Palmatine and Berberine Isolation Artifacts
Name in Czech Izolační artefakty berberinu a palmatinu
Authors MAREK, Radek (203 Czech Republic, guarantor, belonging to the institution), Pavlína SEČKÁŘOVÁ (203 Czech Republic, belonging to the institution), Dagmar HULOVÁ (203 Czech Republic), Jaromír MAREK (203 Czech Republic, belonging to the institution), Jiří DOSTÁL (203 Czech Republic, belonging to the institution) and Vladimír SKLENÁŘ (203 Czech Republic, belonging to the institution).
Edition Journal of Natural Products, American Chemical Society, 2003, 1520-6025.
Other information
Original language English
Type of outcome Article in a journal
Field of Study 10401 Organic chemistry
Country of publisher United States of America
Confidentiality degree is not subject to a state or trade secret
WWW DOI: 10.1021/np0204996
Impact factor Impact factor: 1.849
RIV identification code RIV/00216224:14110/03:00009861
Organization unit Faculty of Medicine
Doi http://dx.doi.org/10.1021/np0204996
UT WoS 000182562800005
Keywords in English alkaloid; isoquinoline; palmatine; berberine; NMR; X-ray; artifact
Tags alkaloid, artifact, berberine, isoquinoline, NMR, palmatine, x-ray
Changed by Changed by: prof. RNDr. Radek Marek, Ph.D., učo 381. Changed: 25/4/2014 17:40.
Abstract
Some 8-substituted derivatives of the protoberberine alkaloids palmatine and berberine have been prepared and investigated by 1D and 2D NMR spectroscopy (H-1, C-13, N-15). Complete NMR data for the 8-hydroxy-, 8-methoxy-, 8-ethoxy-, and 8-trichloromethyl-7,8-dihydro derivatives of palmatine and berberine, as well as X-ray data for 8-methoxydihydroberberine, 8-trichloromethyldihydropalmatine, and 8-trichloromethyldihydroberberine are presented. The physicochemical data for all of these compounds are reviewed and compared with previously published values.
Abstract (in Czech)
BYly připraveny 8-substituované deriváty protoberberinových alkaloidů palmatinu a berberinu a jejich struktura byla zkoumána pomocí 2D NMR spektroskopie a rentgenové strukturní analýzy.
Links
LN00A016, research and development projectName: BIOMOLEKULÁRNÍ CENTRUM
Investor: Ministry of Education, Youth and Sports of the CR, Biomolecular Center
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