| TARABA, Jan and Zdirad ŽÁK. Polysulfonylamines. Bis-(methylsulfonamido) Sulfone, bis-(trifluoromethylsulfonamido) Sulfone, its Synthesis and Crystal Structure. Acta Crystallographica Section C: Crystal Structure. Chester, UK: International Union of Crystallography, C, No 60, p. o79-o81, 3 pp. ISSN 0108-2701. 2004. |
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@article{554907,
author = {Taraba, Jan and Žák, Zdirad},
article_location = {Chester, UK},
article_number = {60},
keywords = {Polysulfonylamines; molecular structure; crystal structure},
language = {eng},
issn = {0108-2701},
journal = {Acta Crystallographica Section C: Crystal Structure},
title = {Polysulfonylamines. Bis-(methylsulfonamido) Sulfone, bis-(trifluoromethylsulfonamido) Sulfone, its Synthesis and Crystal Structure.},
volume = {C},
year = {2004}
}
TY - JOUR
ID - 554907
AU - Taraba, Jan - Žák, Zdirad
PY - 2004
TI - Polysulfonylamines. Bis-(methylsulfonamido) Sulfone, bis-(trifluoromethylsulfonamido) Sulfone, its Synthesis and Crystal Structure.
JF - Acta Crystallographica Section C: Crystal Structure
VL - C
IS - 60
SP - o79-o81
EP - o79-o81
PB - International Union of Crystallography
SN - 01082701
KW - Polysulfonylamines
KW - molecular structure
KW - crystal structure
N2 - Bis(methylsulfamido) sulfone, SO2(NHSO2CH3)2 (1) is synthesized from imido-bis(sulfonylchloride) HN(SO2Cl)2 and bis(trimethylsilyl) methane CH2(Si(CH3)3)2 in trimethylchlorsilane solution. In the solid state there are two independent molecules linked by two N-H....O hydrogen bridges into infinite chains parallel to the b-axis. Bis(trifluoromethylsulfamido)sulfone, SO2(NHSO2CF3)2 (2) is formed by the reaction of trichlorophosphazo-sulfuryl trifuoromethane Cl3PNSO2CF3 with fluorosulfonic acid FSO3H. The molecules are bonded by bifurcated N-H....O bridges into infinite layers parallel to the [001] plane.
ER -
TARABA, Jan and Zdirad ŽÁK. Polysulfonylamines. Bis-(methylsulfonamido) Sulfone, bis-(trifluoromethylsulfonamido) Sulfone, its Synthesis and Crystal Structure. \textit{Acta Crystallographica Section C: Crystal Structure}. Chester, UK: International Union of Crystallography, C, No~60, p.~o79-o81, 3 pp. ISSN~0108-2701. 2004.
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