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@inproceedings{566527, author = {Bartoš, Petr and Mazal, Ctibor}, address = {Praha}, booktitle = {Chemické listy}, keywords = {bicyclopentanes; staffanes; cyclodextrin; NMR}, language = {eng}, location = {Praha}, pages = {41-42}, publisher = {Česká společnost chemická}, title = {Inclusion complexes between 3,3-substituted [n]staffanes and beta-cyclodextrin in water.}, url = {http://www.vscht.cz/chem_listy/}, year = {2004} }
TY - JOUR ID - 566527 AU - Bartoš, Petr - Mazal, Ctibor PY - 2004 TI - Inclusion complexes between 3,3-substituted [n]staffanes and beta-cyclodextrin in water. PB - Česká společnost chemická CY - Praha KW - bicyclopentanes KW - staffanes KW - cyclodextrin KW - NMR UR - http://www.vscht.cz/chem_listy/ N2 - Axially substituted [n]staffanes I form inclusion complexes with beta-cyclodextrin (II) in water. 1H NMR spectrum of a water solution of â-cyclodextrin II has shown apparent changes of chemical shifts of intracavity protons H-3 and H-5 upon addition of [2]staffane-3,3-diol (Ia)into the solution. Nuclear Overhauser effect has been observed between beta-cyclodextrin protons H-3, H-5 and bridge protons of the diol Ia. The method of continuous variations applied to the both complexation sensitive chemical shifts revealed formation of host-guest complex of 1:1 stoichiometry. ER -
BARTOŠ, Petr a Ctibor MAZAL. Inclusion complexes between 3,3-substituted [n]staffanes and beta-cyclodextrin in water. In \textit{Chemické listy}. Praha: Česká společnost chemická. s.~41-42, 1 s. ISSN~0009-2770. 2004.
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