Detailed Information on Publication Record
2004
Liquid chromatographic-mass spectrometric determination of genistin and daidzin in soybean food samples after accelerated solvent extraction with modified content of extraction cell.
KLEJDUS, Bořivoj, Radka MIKELOVÁ, Vojtěch ADAM, Josef ZEHNÁLEK, Jan VACEK et. al.Basic information
Original name
Liquid chromatographic-mass spectrometric determination of genistin and daidzin in soybean food samples after accelerated solvent extraction with modified content of extraction cell.
Name in Czech
HPLC/MS stanovení genistinu a daidzinu v potravinách na bázi sojových bobů
Name (in English)
Liquid chromatographic-mass spectrometric determination of genistin and daidzin in soybean food samples after accelerated solvent extraction with modified content of extraction cell.
Authors
KLEJDUS, Bořivoj (203 Czech Republic), Radka MIKELOVÁ (203 Czech Republic), Vojtěch ADAM (203 Czech Republic, guarantor), Josef ZEHNÁLEK (203 Czech Republic), Jan VACEK (203 Czech Republic), René KIZEK (203 Czech Republic) and Vlastimil KUBÁŇ (203 Czech Republic)
Edition
Analytica Chimica Acta, 2004, 0003-2670
Other information
Language
Czech
Type of outcome
Článek v odborném periodiku
Field of Study
10406 Analytical chemistry
Country of publisher
Czech Republic
Confidentiality degree
není předmětem státního či obchodního tajemství
Impact factor
Impact factor: 2.588
RIV identification code
RIV/00216224:14310/04:00011143
Organization unit
Faculty of Science
UT WoS
000222494200001
Keywords in English
accelerated solvent extraction; daidzin; foodstuffs; genistin; high-performance liquid chromatography; isoflavones; mass spectrometry; solvent extraction; Soxhlet extraction; soybean food; ultrasonic extraction; UV spectrophotometric detection
Tags
Změněno: 22/5/2009 21:59, prof. RNDr. Vojtěch Adam, Ph.D.
V originále
A newly elaborated accelerated solvent extraction (ASE) procedure allowed more accurate (<2%) and precise (<5-8% rel.) HPLC/UV/MS determination of isoflavones in different kinds of food made from soybean (products of ecological agriculture), i.e. soy farina, soy meat granulate, soy meat laminae, soy meat bits, Protmix and EKO-B1. The on-column limits of detection (LOD) for daidzin/genistin were 1.2/1.6 fmol for the signal-to-noise ratio S/N = 3 and 1-3 fmol for daidzem, genistein, formononetin, biochanin A and ononin, respectively. Final concentrations of daidzin in soybean foods fluctuated between 30 and 60 mug/g of dry matter (DM). Significantly higher concentrations of genistin (between 60 and 130 mug/g DM) were found in the soybean foods.
In English
A newly elaborated accelerated solvent extraction (ASE) procedure allowed more accurate (<2%) and precise (<5-8% rel.) HPLC/UV/MS determination of isoflavones in different kinds of food made from soybean (products of ecological agriculture), i.e. soy farina, soy meat granulate, soy meat laminae, soy meat bits, Protmix and EKO-B1. The on-column limits of detection (LOD) for daidzin/genistin were 1.2/1.6 fmol for the signal-to-noise ratio S/N = 3 and 1-3 fmol for daidzem, genistein, formononetin, biochanin A and ononin, respectively. Final concentrations of daidzin in soybean foods fluctuated between 30 and 60 mug/g of dry matter (DM). Significantly higher concentrations of genistin (between 60 and 130 mug/g DM) were found in the soybean foods.
Links
| MSM 432100001, plan (intention) |
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