HELFEN, L., F. DEHN, Petr MIKULÍK and T. BAUMBACH. Three-dimensional imaging of cement microstructure evolution during hydration Three-dimensional imaging of cement microstructure evolution during hydration. Advances in Cement Research. London, 2005, vol. 17, No 3, p. 103-111. ISSN 0951-7197.
Other formats:   BibTeX LaTeX RIS
Basic information
Original name Three-dimensional imaging of cement microstructure evolution during hydration Three-dimensional imaging of cement microstructure evolution during hydration
Name in Czech Třírozměrné zobrazení vývoje mikrostruktury cementu během jeho tuhnutí
Authors HELFEN, L. (276 Germany), F. DEHN (276 Germany), Petr MIKULÍK (203 Czech Republic, guarantor) and T. BAUMBACH (276 Germany).
Edition Advances in Cement Research, London, 2005, 0951-7197.
Other information
Original language English
Type of outcome Article in a journal
Field of Study 10302 Condensed matter physics
Country of publisher United Kingdom of Great Britain and Northern Ireland
Confidentiality degree is not subject to a state or trade secret
WWW URL
Impact factor Impact factor: 0.500
RIV identification code RIV/00216224:14310/05:00014831
Organization unit Faculty of Science
UT WoS 000231747900002
Keywords in English cement; concrete; hydration; microtomography; synchrotron radiation
Tags cement, concrete, Hydration, microtomography, synchrotron radiation
Tags International impact, Reviewed
Changed by Changed by: doc. RNDr. Petr Mikulík, Ph.D., učo 855. Changed: 12/2/2007 18:35.
Abstract
Synchrotron radiation is used for X-ray computed tomography to characterise the hydration process of Portland cement. Quantitative determination of the three-dimensional absorption coefficient distribution due to the use of monochromatic radiation and the achieved high spatial resolution allows the study of the spatial microstructure of cement volume during hydration. The present study has demonstrated the potential of the method for real-time imaging of the evolution of cement structure after solidification. The method yields three-dimensional (3-D) images of the sample volume in a non-destructive manner. Thus, by reiterated imaging of the same sample region at different times, processes in the sample volume can be tracked. During cement hydration, effects such as the formation and further evolution of microcracks and pores mainly related to autogeneous shrinkage could be observed for the first time in the cement volume with up to 1 micrometre resolution. Image analysis of the acquired 3-D data sets allows the determination of the temporal evolution of microporosity and of the fraction of contiguous pore volume for different water : cement ratios of the initial cement paste.
Abstract (in Czech)
Synchrotronové záření je použito pro rtg výpočetní tomografii (CT) k charakterizaci hydratačního procesu portlandského cementu. Kvalitativní určení rozložení koeficientu absorbce ve 3D bylo umožněno použitím monochromatického záření. Získané vysoké rozlišení umožnilo získat velké prostorové rozlišení v objemu tvrdnoucího cementu během hydratace a to i při nedestruktivním měření v reálném čase. Kvalitativní analýzou bylo možné sledovat stejnou část objemu a jeho vývoj v čase. Poprvé bylo možné studovat vytváření a vývoj efektů jako jsou mikrotrhliny a póry ve velikosti s rozlišením až do 1 mikrometru. Analýza mikroporozity byla provedena pro sérii vzorků s různým objemem mezi vodou a cementovou pastou.
Links
MSM0021622410, plan (intention)Name: Fyzikální a chemické vlastnosti pokročilých materiálů a struktur
Investor: Ministry of Education, Youth and Sports of the CR, Physical and chemical properties of advanced materials and structures
PrintDisplayed: 7/10/2024 21:25