ŠVÁBENSKÝ, Radim, Michal ORAVEC and Zdeněk ŠIMEK. Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry. International Journal of Environmental analytical cemistry. 2009, Vol. 89, No. 3, p. 167-181. ISSN 0306-7319.
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Basic information
Original name Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry
Name in Czech Stanovení polycyklických aromatických dusíkatých heterocyklů pomocí kapalinové chromatografie s tandemovou hmotnostní detekcí.
Authors ŠVÁBENSKÝ, Radim (203 Czech Republic), Michal ORAVEC (203 Czech Republic) and Zdeněk ŠIMEK (203 Czech Republic, guarantor).
Edition International Journal of Environmental analytical cemistry, 2009, 0306-7319.
Other information
Original language English
Type of outcome Article in a journal
Field of Study 10406 Analytical chemistry
Country of publisher United Kingdom of Great Britain and Northern Ireland
Confidentiality degree is not subject to a state or trade secret
Impact factor Impact factor: 1.703
RIV identification code RIV/00216224:14310/09:00036101
Organization unit Faculty of Science
UT WoS 000263288600003
Keywords in English polycyclic aromatic nitrogen heterocycles; PANHs; soil; LC-ESI/MS/MS
Tags LC-ESI/MS/MS, PANHs, Polycyclic Aromatic Nitrogen Heterocycles, soil
Tags International impact, Reviewed
Changed by Changed by: doc. RNDr. Zdeněk Šimek, CSc., učo 37019. Changed: 8/3/2010 22:43.
Abstract
Development of LC/MS/MS method for analysing polycyclic aromatic nitrogen hydrocarbons (PANHs) in soil samples is presented. Optimisation of individual chromatographic/mass spectrometric conditions was made in order to obtain a method for the determination of 15 PANHs content in an organic extract from the soil. Detection limits (LOD) in the range of 0.3 to 15 pg per injection were 15 obtained for individual PANHs. LC/MS/MS method has a lower LOD value compared to LC/DAD/FLD methods in general. Developed LC/MS/MS method was used for determination of PANHs content in soil samples collected in contaminated areas of the southeast region of the Czech Republic. Highest concentrations of PANHs have been found in the samples collected in the immediate vicinity of the industrial basin. Concentrations of the contaminants in samples collected in surrounding villages were higher compared to the sample collected in clean area of the Czech Republic.
Abstract (in Czech)
Development of LC/MS/MS method for analysing polycyclic aromatic nitrogen hydrocarbons (PANHs) in soil samples is presented. Optimisation of individual chromatographic/mass spectrometric conditions was made in order to obtain a method for the determination of 15 PANHs content in an organic extract from the soil. Detection limits (LOD) in the range of 0.3 to 15 pg per injection were 15 obtained for individual PANHs. LC/MS/MS method has a lower LOD value compared to LC/DAD/FLD methods in general. Developed LC/MS/MS method was used for determination of PANHs content in soil samples collected in contaminated areas of the southeast region of the Czech Republic. Highest concentrations of PANHs have been found in the samples collected in the immediate vicinity of the industrial basin. Concentrations of the contaminants in samples collected in surrounding villages were higher compared to the sample collected in clean area of the Czech Republic.
Links
MSM0021622412, plan (intention)Name: Interakce mezi chemickými látkami, prostředím a biologickými systémy a jejich důsledky na globální, regionální a lokální úrovni (INCHEMBIOL) (Acronym: INCHEMBIOL)
Investor: Ministry of Education, Youth and Sports of the CR, Interactions among the chemicals, environment and biological systems and their consequences on the global, regional and local scales (INCHEMBIOL)
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