COBO, Marcio Fernando, Kateřina MALIŇÁKOVÁ, Detlef REICHERT, Kay SAALWÄCHTER and Eduardo Ribeiro DEAZEVEDO. Intermediate motions and dipolar couplings as studied by Lee-Goldburg cross-polarization NMR: Hartmann-Hahn matching profiles. Physical Chemistry Chemical Physics. Great Britain: ROYAL SOC CHEMISTRY, 2009, vol. 11, No 32, p. 7036-7047. ISSN 1463-9076. |
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@article{842288, author = {Cobo, Marcio Fernando and Maliňáková, Kateřina and Reichert, Detlef and Saalwächter, Kay and deAzevedo, Eduardo Ribeiro}, article_location = {Great Britain}, article_number = {32}, keywords = {Lee-Goldburg cross-polarization; molecular motion in the intermediate regime; Hartmann-Hahn matching profiles; heteronuclear dipolar coupling}, language = {eng}, issn = {1463-9076}, journal = {Physical Chemistry Chemical Physics}, title = {Intermediate motions and dipolar couplings as studied by Lee-Goldburg cross-polarization NMR: Hartmann-Hahn matching profiles}, volume = {11}, year = {2009} }
TY - JOUR ID - 842288 AU - Cobo, Marcio Fernando - Maliňáková, Kateřina - Reichert, Detlef - Saalwächter, Kay - deAzevedo, Eduardo Ribeiro PY - 2009 TI - Intermediate motions and dipolar couplings as studied by Lee-Goldburg cross-polarization NMR: Hartmann-Hahn matching profiles JF - Physical Chemistry Chemical Physics VL - 11 IS - 32 SP - 7036-7047 EP - 7036-7047 PB - ROYAL SOC CHEMISTRY SN - 14639076 KW - Lee-Goldburg cross-polarization KW - molecular motion in the intermediate regime KW - Hartmann-Hahn matching profiles KW - heteronuclear dipolar coupling N2 - The use of simple Lee-Goldburg cross-polarization (LG-CP) NMR experiments for obtaining quantitative information of molecular motion in the intermediate regime is evaluated. In particular, measurement of Hartmann-Hahn matching profiles for the assessment of heteronuclear dipolar couplings as well as dynamics is introduced as an alternative to the more common analysis of build-up curves. ER -
COBO, Marcio Fernando, Kateřina MALIŇÁKOVÁ, Detlef REICHERT, Kay SAALWÄCHTER and Eduardo Ribeiro DEAZEVEDO. Intermediate motions and dipolar couplings as studied by Lee-Goldburg cross-polarization NMR: Hartmann-Hahn matching profiles. \textit{Physical Chemistry Chemical Physics}. Great Britain: ROYAL SOC CHEMISTRY, 2009, vol.~11, No~32, p.~7036-7047. ISSN~1463-9076.
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