Investigation of the osteitis deformans phases in snake vertebrae by double-pulse laser-induced breakdown spectroscopy

GALIOVÁ, Michaela, Jozef KAISER, Karel NOVOTNÝ, Martin IVANOV, Miriam NÝVLTOVÁ FIŠÁKOVÁ, Lucia MANCINI, Giuliana TROMBA, Tomáš VACULOVIČ, Miroslav LIŠKA and Viktor KANICKÝ. Investigation of the osteitis deformans phases in snake vertebrae by double-pulse laser-induced breakdown spectroscopy. ANALYTICAL AND BIOANALYTICAL CHEMISTRY. HEIDELBERG, GERMANY: SPRINGER-VERLAG HEIDELBERG, 2010, vol. 398, No 2, p. 1095-1107. ISSN 1618-2642. Available from: https://dx.doi.org/10.1007/s00216-010-3976-1.

Basic information

• Original name: Investigation of the osteitis deformans phases in snake vertebrae by double-pulse laser-induced breakdown spectroscopy
• Name in Czech: Analýza Osteitis deformans na hadich obratlech pomocí dvoupulzní spektroskopie laserem indukovaného mikroplazmatu
• Authors: GALIOVÁ, Michaela (203 Czech Republic, belonging to the institution), Jozef KAISER (203 Czech Republic), Karel NOVOTNÝ (203 Czech Republic, guarantor, belonging to the institution), Martin IVANOV (203 Czech Republic, belonging to the institution), Miriam NÝVLTOVÁ FIŠÁKOVÁ (203 Czech Republic), Lucia MANCINI (380 Italy), Giuliana TROMBA (380 Italy), Tomáš VACULOVIČ (203 Czech Republic, belonging to the institution), Miroslav LIŠKA (203 Czech Republic) and Viktor KANICKÝ (203 Czech Republic, belonging to the institution).
• Edition: ANALYTICAL AND BIOANALYTICAL CHEMISTRY, HEIDELBERG, GERMANY, SPRINGER-VERLAG HEIDELBERG, 2010, 1618-2642.

Other information

• Original language: English
• Type of outcome: Article in a journal
• Field of Study: 10406 Analytical chemistry
• Country of publisher: Czech Republic
• Confidentiality degree: is not subject to a state or trade secret
• Impact factor: Impact factor: 3.841
• RIV identification code: RIV/00216224:14310/10:00051493
• Organization unit: Faculty of Science
• Doi: http://dx.doi.org/10.1007/s00216-010-3976-1
• UT WoS: 000281842400047
• Keywords (in Czech): Laserová ablace; LIBS; mapování; X-ray mikrotomografie; fosilie; hadí obratle
• Keywords in English: Laser ablation; LIBS; Mapping; X-ray microtomography; Fossil; Snake vertebra
• Tags: AKb, rivok

Abstract

Double-pulse laser-induced breakdown spectroscopy (DP-LIBS) was optimized for microspatial analyses of fossil and recent snake vertebrae. As complimentary techniques, solution analysis by inductively coupled plasma mass spectrometry and synchrotron radiation X-ray microtomography was utilized in order to determine the overall concentration of the selected elements in the samples and to visualize nondestructively the fossil sample microstructure,respectively. Elemental mapping of pathological bony tissue by DP-LIBS has been proven as a powerful tool for considering the osteitis deformans phases in fossil vertebrae.

Abstract (in Czech)

Metoda dvoupulzní spektroskopie laserem indukovaného mikroplazmatu (DP-LIBS) byla optimalizována pro prvkové mapování fosilních a recentních vzorků hadích obratlů. Pro zjištění celkového obsahu vybraných prvků byla provedena roztoková analýza pomocí hmotnostní spektrometrie s indukčně vázaným plazmatem a mikrostruktura vzorku byla zkoumána pomocí X-ray mikrotomografie. Prvkové mapovaní patologické kostní tkáně provedené metodou DP-LIBS bylo použito pro sledování sledování fází onemocnění osteitis deformans.

Links

• ME08002, research and development project: Name: Použití spektroskopie laserem buzeného plazmatu (LIBS) a laserové ablace ve spojení s ICP-OES/MS spektroskopií pro chemické mapování biominerálů

Investor: Ministry of Education, Youth and Sports of the CR, Utilization of the laser induced breakdown spectroscopy (LIBS) and laser ablation ICP-OES/MS spectroscopy for chemical mapping of biominerals, Research and Development Programme KONTAKT (ME)

• MSM0021622411, plan (intention): Name: Studium a aplikace plazmochemických reakcí v neizotermickém nízkoteplotním plazmatu a jeho interakcí s povrchem pevných látek

Investor: Ministry of Education, Youth and Sports of the CR, Study and application of plasma chemical reactions in non-isothermic low temperature plasma and its interaction with solid surface

• MSM0021622412, plan (intention): Name: Interakce mezi chemickými látkami, prostředím a biologickými systémy a jejich důsledky na globální, regionální a lokální úrovni (INCHEMBIOL) (Acronym: INCHEMBIOL)

Investor: Ministry of Education, Youth and Sports of the CR, Interactions among the chemicals, environment and biological systems and their consequences on the global, regional and local scales (INCHEMBIOL)