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@inproceedings{975522,
author = {Zelina, Peter and Jašek, Ondřej and Kudrle, Vít and David, Bohumil and Pizúrová, Naděžda},
address = {Shanghai, China},
booktitle = {Proceedings of ICCE 19},
editor = {David Hui},
keywords = {Plasma synthesis; PECVD; Nanoparticle; Magnetic nanopowder; Iron oxide},
language = {eng},
location = {Shanghai, China},
pages = {1331-1332},
publisher = {David Hui},
title = {Versatile PECVD process for preparation of iron-based magnetic nanoparticles},
year = {2011}
}
TY - JOUR
ID - 975522
AU - Zelina, Peter - Jašek, Ondřej - Kudrle, Vít - David, Bohumil - Pizúrová, Naděžda
PY - 2011
TI - Versatile PECVD process for preparation of iron-based magnetic nanoparticles
PB - David Hui
CY - Shanghai, China
KW - Plasma synthesis
KW - PECVD
KW - Nanoparticle
KW - Magnetic nanopowder
KW - Iron oxide
N2 - Using microwave low-pressure discharge, we synthesised magnetic iron-oxide nanopowder from the iron pentacarbonyl precursor. We were able to vary the size and chemical composition (especially the ratio between various iron oxides) by careful control of the process parameters. The nanoparticulate product was analysed by X-ray diffraction (XRD) and Raman spectroscopy. However, the XRD cannot reliably distinguish between the size-broadened peaks of gamma-Fe2O3 (maghemite) and Fe3O4 (magnetite) due to their nearly identical crystalline structure. Hence we used a chemical method to determine the presence of Fe(II) and Fe(III) ions in the nanopowder samples. The results agree with those from the Raman spectroscopy.
ER -
ZELINA, Peter, Ondřej JAŠEK, Vít KUDRLE, Bohumil DAVID and Naděžda PIZÚROVÁ. Versatile PECVD process for preparation of iron-based magnetic nanoparticles. In David Hui. \textit{Proceedings of ICCE 19}. Shanghai, China: David Hui, 2011, p.~1331-1332.
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