J 2012

SILVER NANOPARTICLES SINTERING AT LOW TEMPERATURE ON A COPPER SUBSTRATE: IN SITU CHARACTERISATION UNDER INERT ATMOSPHERE AND AIR

SOPOUŠEK, Jiří, Jiří BURŠÍK, Jakub ZÁLEŠÁK and Zbyněk PEŠINA

Basic information

Original name

SILVER NANOPARTICLES SINTERING AT LOW TEMPERATURE ON A COPPER SUBSTRATE: IN SITU CHARACTERISATION UNDER INERT ATMOSPHERE AND AIR

Name in Czech

Nizkoteplotní sintrace nanostříbra na substrátu mědi: In situ charakterizace za inertní atmosféry a na vzduchu

Authors

SOPOUŠEK, Jiří (203 Czech Republic, guarantor, belonging to the institution), Jiří BURŠÍK (203 Czech Republic), Jakub ZÁLEŠÁK (203 Czech Republic, belonging to the institution) and Zbyněk PEŠINA (203 Czech Republic)

Edition

Journal of Mining and Metallurgy B, Bor, Serbia, Faculty of Metallurgy, Bor, 2012, 1450-5339

Other information

Language

English

Type of outcome

Článek v odborném periodiku

Field of Study

20000 2. Engineering and Technology

Country of publisher

Serbia

Confidentiality degree

není předmětem státního či obchodního tajemství

Impact factor

Impact factor: 1.435

RIV identification code

RIV/00216224:14740/12:00057393

Organization unit

Central European Institute of Technology

UT WoS

000300798900007

Keywords (in Czech)

Thermal analysis; Silver; copper; DSC; electrical resistance; heat of sintering

Keywords in English

Termická analýza; stříbro; měď; DSC; elektrická vodivost; teplo sintrace

Tags

International impact, Reviewed
Změněno: 12/4/2013 09:15, Olga Křížová

Abstract

V originále

Silver nanoparticles (Ag-NPs) were prepared by wet synthesis. The Ag-NPs suspension and the copper substrate plate were used for a preparation of substrate-nanoparticle-substrate samples. The sandwich like samples Cu/Ag/Cu were prepared and investigated in-situ at the isothermal external conditions (IEC) and inside apparatus for simultaneous thermal analysis STA409. The in-situ results of the electrical resistance were recorded during the Cu/Ag/Cu (IEC) sample preparation and heat treatment. Thermal effects of the Ag-NPs sintering between copper substrates were measured by differential scanning calorimetry (DSC) under different atmospheres. The prepared Cu/Ag/Cu sandwich samples were characterised by means of both optical and electron microscopy. The process of the low temperature sintering of the Ag-NPs was monitored using both thermogravimetry (TG) and DSC technique inside calorimeter under inert gas and under synthetic air. The exothermic heat effect of nanosilver sintering was evaluated.

In Czech

Ag nano bylo připraveno mokrou syntézou. Byly připraveny sendvičové vzorky Cu/AG-NANO/Cu. Byl měřen tepelný efekt sintrace v DSC metodou v kalorimetru. Sintrace byla sledována pod inertním plynem a v argonu.

Links

ED1.1.00/02.0068, research and development project
Name: CEITEC - central european institute of technology
GA106/09/0700, research and development project
Name: Termodynamika a mikrostruktura nanopráškových pájek šetrných k životnímu prostředí
Investor: Czech Science Foundation, Thermodynamics and microstructure of environmentally friendly nanoparticle solders
GD106/09/H035, research and development project
Name: Víceúrovňový design pokrokových materiálů
Investor: Czech Science Foundation
MSM0021622410, plan (intention)
Name: Fyzikální a chemické vlastnosti pokročilých materiálů a struktur
Investor: Ministry of Education, Youth and Sports of the CR, Physical and chemical properties of advanced materials and structures

Files attached

Ag_in_situ_na_Cu_1450-53391200007S.pdf
Request the author's version of the file