FC3016 Laboratory Training in Analytical Chemistry

Faculty of Education
Spring 2020
Extent and Intensity
0/0/2. 3 credit(s). Type of Completion: k (colloquium).
Teacher(s)
Mgr. Jana Horská, Ph.D. (seminar tutor)
Guaranteed by
Mgr. Jana Horská, Ph.D.
Department of Physics, Chemistry and Vocational Education – Faculty of Education
Contact Person: Jana Jachymiáková
Supplier department: Department of Physics, Chemistry and Vocational Education – Faculty of Education
Timetable of Seminar Groups
FC3016/01: Tue 18. 2. 10:00–13:50 laboratoř 90, Tue 25. 2. 10:00–13:50 laboratoř 90, Tue 3. 3. 10:00–13:50 laboratoř 90, Tue 10. 3. 10:00–13:50 laboratoř 90, Tue 17. 3. 10:00–13:50 laboratoř 90, Tue 24. 3. 10:00–13:50 laboratoř 90, J. Horská
FC3016/02: Wed 19. 2. 8:00–11:50 laboratoř 90, Wed 26. 2. 8:00–11:50 laboratoř 90, Wed 4. 3. 8:00–11:50 laboratoř 90, Wed 11. 3. 8:00–11:50 laboratoř 90, Wed 18. 3. 8:00–11:50 laboratoř 90, Wed 25. 3. 8:00–11:50 laboratoř 90, J. Horská
Prerequisites
Knowledge of general, inorganic and organic chemistry.
Course Enrolment Limitations
The course is only offered to the students of the study fields the course is directly associated with.
fields of study / plans the course is directly associated with
Course objectives
Main objectives can be summarised as follows:
to get basic habits and drafts by executing of analytical processes in analytical laboratory;
to achieve the best accuracy and correctness of results by practical analysis of samples.
Learning outcomes
Upon completion of this course the student will gain:  knowledge of acquiring basic habits and skills in conducting experiments in the analytical laboratory and achieving as accurate and accurate as possible the results of practical analyzes of samples  Skills and skills for performing practical experiments in an analytical laboratory  A comprehensive overview of the content of the subject's subject (Group reactions of cations and anions, Selective reaction of cations and anions, Gravimetry, Volumetric analysis, Instrumental analytical methods).
Syllabus
  • Safety of the work in analytical laboratory. Basic laboratory analytical operations, technics and apparatus.
  • 1. Group reactions of ions. A. Group reactions of cations. B. Group reactions of anions.
  • 2. Selective reactions of cationts.
  • 3. Selective reactions of anions.
  • 4. Gravimetry. A. determination of iron as Fe2O3. B. Determination of nickel with diacetyldioximem.
  • 5. Alcalimetry. A. Standardization of 0,1 mol.dm-3 NaOH solution on oxalate acid. B. Determination of H3PO4. C. Determination of acetic acid in vinegar. D. Determination of amonium nitrogen according Hanuš. E. Potentiometric determination of H3PO4.
  • 6. Acidimetry. A. Standardization of 0,1 mol.dm-3 HCl solution on Na2CO3. B. Determination of Na2CO3 in NaOH according Winkler.
  • 7. Chelatometry. A. Standardization of 0,05 mol.dm-3 chelatone solution. B. Determination of Ca2+ and Mg2+in a mixture. C. Determination of Mg by the titration on eriochrome black T as indicator. D. Determination of Cu2+.
  • 8. Argentometry. A. Standardization of 0,05 mol.dm-3 AgNO3 solution according Mohr or Fajans. B. Determination of Cl- with visual indication of equivalence point. C. Determination of halogenides with potentiometric indication.
  • 9. Permanganate titration and Iodometric titration. A. Standardization of 0,02 mol.dm-3 KMnO4 solution on oxalate acid. B. Determination of Fe2+. C. Standardization of 0,1 mol.dm-3 solution Na2S2O3 on K2Cr2O7. D. Standardization of 0,05 mol.dm-3 solution iodine on Na2S2O3. E. Iodometric determination of ascorbic acid.
  • 10. Spectrophotometry. A. Determination of iron with 1,10-fenanthroline. B. Determination of iron with sulphosalicyle acid. C. Determination of Cd2+ with 4-(2-pyridylazo)-resorcine. D. Determination of NO3- after reduction on NO2- with sulphanile acid and N-(1-naftyl)-ethylendiamine dihydrochloride. E. Determination of β-carotene.
  • 11. Chromatography on thin layer – separation of mixtures of food dyes.
  • 12. Evaluation of results of laboratory exercises – computer programs.
Literature
    required literature
  • Dostál V., Šimek J., Důkaz některých anorganických iontů vybranými analytickými reakcemi, Skripta UP Olomouc, 2. upr. a dopl. vyd. Olomouc 2000. 76 s.
    recommended literature
  • A. Okáč, Analytická chemie kvalitativní, Academia, Praha 1966.
  • JANČÁŘ, L. Analytická chemie. Dostupné z World Wide Web: http://www.is.muni.cz. Viz Studijní materiály předmětu PedF: CH2BP_4P1P.
  • JANČÁŘ, Luděk and Irena JANČÁŘOVÁ. Analytická chemie - laboratorní cvičení (Analytical chemistry - laboratory exercises). Brno: Masarykova univerzita, 1997, 141 pp. ISBN 80-210-1579-9. info
Teaching methods
laboratory exercise
Assessment methods
credit;
written test.
Language of instruction
Czech
Further comments (probably available only in Czech)
Study Materials
The course is taught annually.
Information on the extent and intensity of the course: 8 hodin.
The course is also listed under the following terms Spring 2021, Spring 2022, Spring 2023, Spring 2024, Spring 2025.
  • Enrolment Statistics (Spring 2020, recent)
  • Permalink: https://is.muni.cz/course/ped/spring2020/FC3016