PřF:C7780 Inorganic Materials Chemistry - Course Information

C7780 Inorganic Materials Chemistry

Extent and Intensity

2/0/0. 2 credit(s) (fasci plus compl plus > 4). Recommended Type of Completion: zk (examination). Other types of completion: k (colloquium).

Teacher(s)

prof. RNDr. Jiří Pinkas, Ph.D. (lecturer)

Guaranteed by

prof. RNDr. Jiří Pinkas, Ph.D.
Chemistry Section – Faculty of Science

Timetable

Thu 16:00–17:50 03021

Prerequisites

Thorough knowledge of principles and facts covered by the courses of General, Inorganic, Organic, and Physical Chemistry is required.

Course Enrolment Limitations

The course is also offered to the students of the fields other than those the course is directly associated with.

fields of study / plans the course is directly associated with

there are 25 fields of study the course is directly associated with, display

Course objectives

This course covers the basic principles of Materials Chemistry with the emphasis on inorganic materials. The lecture focuses on the relation between structure and propertis of materials. Synthetic methods are grouped according to the physical state of reactants: solid, liquid, and gaseous. Fabrication methods of different shapes are also covered.

Syllabus

• 1. Introduction, Materials Science, Materials Chemistry, Chemical Synthesis of Materials.
  2. Physicochemical Methods of Materials Characterization.
  3. Basic Inorganic Structure Types. Metals, Ionic, and Covalent Compounds. Defects.
  4. Electronic Structure of Solids, Chemical Bonding, Band Theory.
  5. Electrical, Mechanical, Thermal, Optical, Magnetic Properties of Materials.
  6. Direct Reaction of Solids, Synthesis of Spinel, Kirkendall Ratio.
  7. Carbothermal Reduction, Self-Sustaining Reactions, Combustion Reactions, Polymer Pyrolysis, Mechanochemical Synthesis, Microwave-Assisted Synthesis.
  8. Dry High-Pressure Methods, Detonation Reactions, Diamond Synthesis, Hard Materials.
  9. Vapor Phase Transport, Aerosol Routes, Flame Hydrolysis.
  10. Precursor Methods, Flux or Molten Salt Method, Ionic Liquids, Sonochemical Synthesis.
  11. Sol-Gel Methods, Hydrothermal Synthesis.
  12. Zeolites, Mesoporous Materials, Layered Materials, Intercalation.
  13. Growth of Single Crystals.
  14. Synthesis of Thin Films, Chemical Vapor Deposition, Self-Assembled Monolayers.
  15. Nanostructured Materials.

Literature

• SCHUBERT, Ulrich and Nicola HÜSING. Synthesis of Inorganic Materials. Weinheim: Wiley-VCH, 2000, 396 pp. ISBN 3-527-29550-X. info
• MÜLLER, Ulrich. Inorganic Structural Chemistry. 2nd ed. John Wiley & Sons., 1993. ISBN 0-471-93717-7. info
• CALLISTER, William D., Jr. Materials Science and Engineering, An Introduction. 4th ed. John Wiley and Sons, 1997. ISBN 0-471-13459-7. info
• SMART, Lesley and Elaine MOORE. Solid state chemistry : an introduction. 2nd ed. London: Chapman & Hall, 1995, xiv, 379 s. ISBN 0-412-62220-3. info
• SEGAL, David. Chemical Synthesis of Advanced Ceramic Materials. Cambridge, UK: Cambridge University Press, 1989. ISBN 0-521-35436-6. info
• INTERRANTE, L. V. and M. J. HAMPDEN-SMITH. Chemistry of Advanced Materials, An Overview. New York: Wiley-VCH, 1998. ISBN 0-471-18590-6. info
• BRUCE, D. W. and D. O'HARE. Inorganic Materials. Chichester: John Wiley & Sons, 1997. ISBN 0-471-96036-5. info
• YANAGIDA, H., K. KUNIHITO, M. MIYAYAMA and H. YAMADA. The Chemistry of Ceramics. John wiley & Sons, 1996. ISBN 0-471-96733-5. info
• HOFFMANN, Roald. Solids and Surfaces. New York: VCH Publishers, 1988. ISBN 0-89573-709-4. info
• KODAS, T. and M. HAMPDEN-SMITH. The Chemistry of Metal CVD. Weinheim: VCH Weinheim, 1994. ISBN 3-527-29071-0. info
• KRATOCHVÍL, Bohumil. Chemie a fyzika pevných látek 1. Praha: Vysoká škola chemicko-technologická, 1994, 233 s. ISBN 80-7080-196-4. info
• KRATOCHVÍL, Bohumil. Základy fyziky a chemie pevných látek II. Praha: Vysoká škola chemicko-technologická, 1990, 160 s. ISBN 80-7080-055-0. info
• MASON, Timothy J and John P LORIMER. Applied Sonochemistry. Weinheim: Wiley-VCH, 2002, 303 pp. ISBN 3-527-30205-0. info
• WEST, Anthony R. Basic Solid State Chemistry. Second Edition. Chichester: John Wiley & Sons, 1999. ISBN 0-471-987565-5. info
• MASON, Timothy J. Sonochemistry. Oxford: Oxford University Press, 1999, 92 pp. Oxford Chemistry Primers. ISBN 0-19-850371-7. info
• GIROLAMI, Gregory S., Thomas B. RAUCHFUSS and Robert J. ANGELICI. Synthesis and technique in inorganic chemistry :a laboratory manual. 3rd ed. Sausalito, Calif.: University Science Books, 1998, xiii, 272. ISBN 0-935702-48-2. info
• HOLZAPFEL, Wilfried B and Neil S ISAACS. High-Pressure Techniques in Chemistry and Physics. Oxford: Oxford University Press, 1997, 388 pp. The Practical Approach in Chemistry Series. ISBN 0-19-855811-2. info
• JENKINS, Ron and Robert L. SNYDER. Introduction to X-ray powder diffractometry. New York: John Wiley & Sons, 1996, xxiii, 403. ISBN 0471513393. info
• WELLER, Mark. Inorganic Materials Chemistry. Oxford, UK: Oxford University Press, 1994. ISBN 0-19-855799-X. info
• CHEETHAM, A K and Peter DAY. Solid State Chemistry - Compounds. Oxford: Oxford University Press, 1992, 304 pp. ISBN 0-19-855166-5. info
• CHEETHAM, A K and Peter DAY. Solid State Chemistry - Techniques. Oxford: Oxford University Press, 1987, 398 pp. ISBN 0-19-855286-6. info

Assessment methods (in Czech)

14 lectures, 3 graded homeworks, 1 short presentation, written final exam

Language of instruction

English

Follow-Up Courses

• C6750 Materials Chemistry of Metals

Further comments (probably available only in Czech)

The course is taught annually.

Listed among pre-requisites of other courses

• C8870 Synthesis and analysis of new materials
  C7780  
• C8888 Nanochemistry
  C7780  

Teacher's information

http://cheminfo/materials/InorgMater/syllabus.htm

• Enrolment Statistics (Autumn 2005, recent)
  
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