OPTIMISATION OF MECHANICAL PROPERTIES OF NANOLAMINATE COATINGS

a 2015

OPTIMISATION OF MECHANICAL PROPERTIES OF NANOLAMINATE COATINGS

BURŠÍKOVÁ, Vilma, Jiří BURŠÍK, Pavel SOUČEK, Lukáš ZÁBRANSKÝ, Petr VAŠINA et. al.

Základní údaje

Originální název

OPTIMISATION OF MECHANICAL PROPERTIES OF NANOLAMINATE COATINGS

Autoři

BURŠÍKOVÁ, Vilma (203 Česká republika, garant, domácí), Jiří BURŠÍK (203 Česká republika, domácí), Pavel SOUČEK (203 Česká republika, domácí), Lukáš ZÁBRANSKÝ (203 Česká republika, domácí) a Petr VAŠINA (203 Česká republika, domácí)

Vydání

The 15th International Balkan Workshop on Applied Physics, 2015

Další údaje

Jazyk

angličtina

Typ výsledku

Konferenční abstrakt

Obor

10305 Fluids and plasma physics

Stát vydavatele

Rumunsko

Utajení

není předmětem státního či obchodního tajemství

Kód RIV

RIV/00216224:14310/15:00080998

Organizační jednotka

Přírodovědecká fakulta

Klíčová slova anglicky

mechanical properties; nanoindentation; modulus mapping

Změněno: 5. 9. 2015 17:01, Mgr. Lukáš Zábranský, Ph.D.

Anotace

V originále

Recently, there has been an increased interest in boron and carbon based films with X2BC composition. Theoretical ab-initio models predict unusual combination of high stiffness and moderate ductility for these types of films when X=Ta, Mo or W. The aim of the present work was to prepare thin Mo2BC films at different deposition temperatures using magnetron sputtering technique and to evaluate the dependence of their mechanical properties on the deposition parameters. The film structure and composition were studied using X-ray diffraction technique, XPS and Ruthefor Backscattered Spectroscopy combined with Elastic Recoil Detection Analysis. The microstructure of layers was studied using a Tescan LYRA 3XMU SEM×FIB scanning electron microscope (SEM), a Philips CM12 STEM transmission electron microscope (TEM) and a JEOL 2100F high resolution TEM. The quasistatic and dynamic nanoindentation response of the films was studied using wide range of testing conditions. The friction coefficient, sratch and wear resistance of the coatings were studied using nanoscratch and nanowear tests. The fracture toughness of the coatings was evaluated using nano and microindentation techniques. The modulus mapping capability was applied to obtain quantitative maps of the storage and loss stiffness and the storage and loss modulus. The modulus mapping combines the in-situ imaging capabilities with the ability to perform nanodynamic mechanical analysis. In Fig. 1 an example of the modulus mapping results obtained on nanocomposite MoBC coating is shown. The Czech Science Foundation is acknowledged for the financial support of this work (Project 15-17875S).

Návaznosti

GA15-17875S, projekt VaV

Název: Lokální mikrostrukturní změny vyvolané statickou a dynamickou indentací nanostrukturovaných a nanolaminovaných povlaků

Investor: Grantová agentura ČR, Lokální mikrostrukturní změny vyvolané statickou a dynamickou indentací nanostrukturovaných a nanolaminovaných povlaků

Citovat

BURŠÍKOVÁ, Vilma, Jiří BURŠÍK, Pavel SOUČEK, Lukáš ZÁBRANSKÝ a Petr VAŠINA. OPTIMISATION OF MECHANICAL PROPERTIES OF NANOLAMINATE COATINGS. In The 15th International Balkan Workshop on Applied Physics. 2015.

@proceedings{1309939,
   author = {Buršíková, Vilma and Buršík, Jiří and Souček, Pavel and Zábranský, Lukáš and Vašina, Petr},
   booktitle = {The 15th International Balkan Workshop on Applied Physics},
   keywords = {mechanical properties; nanoindentation; modulus mapping},
   language = {eng},
   title = {OPTIMISATION OF MECHANICAL PROPERTIES OF NANOLAMINATE COATINGS},
   year = {2015}
}

TY  - CONF
ID  - 1309939
AU  - Buršíková, Vilma - Buršík, Jiří - Souček, Pavel - Zábranský, Lukáš - Vašina, Petr
PY  - 2015
TI  - OPTIMISATION OF MECHANICAL PROPERTIES OF NANOLAMINATE COATINGS
KW  - mechanical properties
KW  - nanoindentation
KW  - modulus mapping
N2  - Recently, there has been an increased interest in boron and carbon based films with X2BC composition. Theoretical ab-initio models predict unusual combination of high stiffness and moderate ductility for these types of films when X=Ta, Mo or W. The aim of the present work was to prepare thin Mo2BC films at different deposition temperatures using magnetron sputtering technique and to evaluate the dependence of their mechanical properties on the deposition parameters. The film structure and composition were studied using X-ray diffraction technique, XPS and Ruthefor Backscattered Spectroscopy combined with Elastic Recoil Detection Analysis. The microstructure of layers was studied using a Tescan LYRA 3XMU SEM×FIB scanning electron microscope (SEM), a Philips CM12 STEM transmission electron microscope (TEM) and a JEOL 2100F high resolution TEM. The quasistatic and dynamic nanoindentation response of the films was studied using wide range of testing conditions. The friction coefficient, sratch and wear resistance of the coatings were studied using nanoscratch and nanowear tests. The fracture toughness of the coatings was evaluated using nano and microindentation techniques. The modulus mapping capability was applied to obtain quantitative maps of the storage and loss stiffness and the storage and loss modulus. The modulus mapping combines the in-situ imaging capabilities with the ability to perform nanodynamic mechanical analysis. In Fig. 1 an example of the modulus mapping results obtained on nanocomposite MoBC coating is shown. The Czech Science Foundation is acknowledged for the financial support of this work (Project 15-17875S).
ER  -

BURŠÍKOVÁ, Vilma, Jiří BURŠÍK, Pavel SOUČEK, Lukáš ZÁBRANSKÝ a Petr VAŠINA. OPTIMISATION OF MECHANICAL PROPERTIES OF NANOLAMINATE COATINGS. In \textit{The 15th International Balkan Workshop on Applied Physics}. 2015.

Podrobný výpis o publikaci