Characterization of inner structure of limestone by X-ray
computed sub-micron tomography

J 2018

Characterization of inner structure of limestone by X-ray computed sub-micron tomography

KALASOVÁ, Dominika; Karel DVOŘÁK; Marek SLOBODNÍK; Dalibor VŠIANSKÝ; Tomáš ZIKMUND et. al.

Basic information

Original name

Characterization of inner structure of limestone by X-ray computed sub-micron tomography

Authors

KALASOVÁ, Dominika (203 Czech Republic, guarantor); Karel DVOŘÁK (203 Czech Republic); Marek SLOBODNÍK (203 Czech Republic, belonging to the institution); Dalibor VŠIANSKÝ (203 Czech Republic, belonging to the institution); Tomáš ZIKMUND (203 Czech Republic); Jiří DLUHOŠ (203 Czech Republic); Rostislav VÁŇA (203 Czech Republic); Jaroslav BUREŠ (203 Czech Republic) and Jozef KAISER (203 Czech Republic)

Edition

Construction and Building Materials, OXFORD, ELSEVIER SCI LTD, 2018, 0950-0618

Other information

Language

English

Type of outcome

Article in a journal

Field of Study

20501 Materials engineering

Country of publisher

United Kingdom of Great Britain and Northern Ireland

Confidentiality degree

is not subject to a state or trade secret

Impact factor

Impact factor: 4.046

RIV identification code

RIV/00216224:14310/18:00106498

Organization unit

Faculty of Science

DOI

https://doi.org/10.1016/j.conbuildmat.2018.04.142

UT WoS

000433656300066

EID Scopus

2-s2.0-85046474212

Keywords in English

Limestone; Petrography; X-ray computed tomography; Fluid inclusions; Microthermometry

Abstract

In the original language

Limestones are fundamental industrial and building materials. Sparry calcite as a principal petrographic component of limestones can contain fluid inclusions. A certain amount of fluid inclusions directly influences decrepitation which plays an important role in decarbonisation processes. In this paper, a limestone with a high content of fluid inclusions and carbon was investigated. Presence of chlorine and alcalic elements was confirmed with microthermometry, mineralogical and chemical analyses. X-ray computed tomography with sub-micron resolution (CT) was applied to obtain a 3D distribution of cavities. CT data were correlated with some light microscopy images and also with the same sample's tomography data which were gathered using the 3D X-ray energy dispersive spectroscopy (3D EDS) by a scanning electron microscope equipped with a focused ion beam (FIB-SEM). The latter further determined dolomites and metals in the CT data of limestone. (C) 2018 Elsevier Ltd. All rights reserved.

Cite

KALASOVÁ, Dominika; Karel DVOŘÁK; Marek SLOBODNÍK; Dalibor VŠIANSKÝ; Tomáš ZIKMUND; Jiří DLUHOŠ; Rostislav VÁŇA; Jaroslav BUREŠ and Jozef KAISER. Characterization of inner structure of limestone by X-ray computed sub-micron tomography. Construction and Building Materials. OXFORD: ELSEVIER SCI LTD, 2018, vol. 174, June 2018, p. 693-700. ISSN 0950-0618. Available from: https://doi.org/10.1016/j.conbuildmat.2018.04.142.

@article{1503558,
   author = {Kalasová, Dominika and Dvořák, Karel and Slobodník, Marek and Všianský, Dalibor and Zikmund, Tomáš and Dluhoš, Jiří and Váňa, Rostislav and Bureš, Jaroslav and Kaiser, Jozef},
   article_location = {OXFORD},
   article_number = {June 2018},
   doi = {https://doi.org/10.1016/j.conbuildmat.2018.04.142},
   keywords = {Limestone; Petrography; X-ray computed tomography; Fluid inclusions; Microthermometry},
   language = {eng},
   issn = {0950-0618},
   journal = {Construction and Building Materials},
   title = {Characterization of inner structure of limestone by X-ray computed sub-micron tomography},
   volume = {174},
   year = {2018}
}

TY  - JOUR
ID  - 1503558
AU  - Kalasová, Dominika - Dvořák, Karel - Slobodník, Marek - Všianský, Dalibor - Zikmund, Tomáš - Dluhoš, Jiří - Váňa, Rostislav - Bureš, Jaroslav - Kaiser, Jozef
PY  - 2018
TI  - Characterization of inner structure of limestone by X-ray computed sub-micron tomography
JF  - Construction and Building Materials
VL  - 174
IS  - June 2018
SP  - 693-700
EP  - 693-700
PB  - ELSEVIER SCI LTD
SN  - 09500618
KW  - Limestone
KW  - Petrography
KW  - X-ray computed tomography
KW  - Fluid inclusions
KW  - Microthermometry
N2  - Limestones are fundamental industrial and building materials. Sparry calcite as a principal petrographic component of limestones can contain fluid inclusions. A certain amount of fluid inclusions directly influences decrepitation which plays an important role in decarbonisation processes. In this paper, a limestone with a high content of fluid inclusions and carbon was investigated. Presence of chlorine and alcalic elements was confirmed with microthermometry, mineralogical and chemical analyses. X-ray computed tomography with sub-micron resolution (CT) was applied to obtain a 3D distribution of cavities. CT data were correlated with some light microscopy images and also with the same sample's tomography data which were gathered using the 3D X-ray energy dispersive spectroscopy (3D EDS) by a scanning electron microscope equipped with a focused ion beam (FIB-SEM). The latter further determined dolomites and metals in the CT data of limestone. (C) 2018 Elsevier Ltd. All rights reserved.
ER  -

KALASOVÁ, Dominika; Karel DVOŘÁK; Marek SLOBODNÍK; Dalibor VŠIANSKÝ; Tomáš ZIKMUND; Jiří DLUHOŠ; Rostislav VÁŇA; Jaroslav BUREŠ and Jozef KAISER. Characterization of inner structure of limestone by X-ray computed sub-micron tomography. \textit{Construction and Building Materials}. OXFORD: ELSEVIER SCI LTD, 2018, vol.~174, June 2018, p.~693-700. ISSN~0950-0618. Available from: https://doi.org/10.1016/j.conbuildmat.2018.04.142.

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