Synthesis and properties of free-standing graphene nanosheets
at atmospheric pressure conditions

a 2018

Synthesis and properties of free-standing graphene nanosheets at atmospheric pressure conditions

TOMAN, Jozef, Ondřej JAŠEK a Jana JURMANOVÁ

Základní údaje

Originální název

Synthesis and properties of free-standing graphene nanosheets at atmospheric pressure conditions

Název česky

Syntéza a vlastnosti volně stojících nanošupín grafenu za atmosférického tlaku

Autoři

TOMAN, Jozef (703 Slovensko, domácí), Ondřej JAŠEK (203 Česká republika, garant, domácí) a Jana JURMANOVÁ (203 Česká republika, domácí)

Vydání

FEMS Junior EUROMAT 2018, The Main Event for Young Materials Scientists, July 8-12, 2018/Budapest, Hungary, 2018

Další údaje

Jazyk

angličtina

Typ výsledku

Konferenční abstrakt

Obor

10305 Fluids and plasma physics

Stát vydavatele

Maďarsko

Utajení

není předmětem státního či obchodního tajemství

Odkazy

kniha abstraktu

Kód RIV

RIV/00216224:14310/18:00107909

Organizační jednotka

Přírodovědecká fakulta

ISBN

978-963-05-9917-7

Klíčová slova anglicky

graphene; sheets; carbon; microwave; torch discharge

Změněno: 4. 1. 2020 14:53, Mgr. Jozef Toman, Ph.D.

Anotace

V originále

Last decade two-dimensional carbon-based nanostructures such as graphene nanosheets, nanoribbons and carbon nanowalls have attracted much research interest, due to their remarkable properties combining high mechanical strength and flexibility, exceptional electronic and thermal conductivity, high carrier mobility and optical transparency. Potential application in different fields of science and technology include hydrogen and energy storage, reinforcement of polymer composites, electronics, electrochemical devices, or gas sensors. Our deposition process reported in this work is based on injecting ethanol vapours through a microwave plasma environment, where decomposition of ethanol molecules takes place. We used microwave plasma torch discharge (2.45 GHz, ~200 W, Figure 1) operating at atmospheric pressure conditions to synthesize graphene nanosheets with rectangular shape and typical size of hundreds of nanometres. Argon flowing through the central channel of the nozzle was used as the working gas to ignite the discharge. Mixture consisting of ethanol vapours and additional argon flow was delivered into plasma environment by outer channel of the nozzle. Wide range of deposition conditions resulted in synthesis of different types of carbon material. However, mastering the deposition process by setting specific set of deposition conditions led to synthesis of graphene sheets (Figure 2). Created samples were analysed by scanning electron microscopy, Raman spectroscopy and X-ray photoelectron spectroscopy to probe the morphological, chemical and microstructural features of the produced material.

Návaznosti

GA18-08520S, projekt VaV

Název: Studium procesu nukleace dvourozměrných uhlíkových nanostruktur v mikrovlnném plazmatu

Investor: Grantová agentura ČR, Studium procesu nukleace dvourozměrných uhlíkových nanostruktur v mikrovlnném plazmatu

Citovat

TOMAN, Jozef, Ondřej JAŠEK a Jana JURMANOVÁ. Synthesis and properties of free-standing graphene nanosheets at atmospheric pressure conditions. In FEMS Junior EUROMAT 2018, The Main Event for Young Materials Scientists, July 8-12, 2018/Budapest, Hungary. 2018. ISBN 978-963-05-9917-7.

@proceedings{1597937,
   author = {Toman, Jozef and Jašek, Ondřej and Jurmanová, Jana},
   booktitle = {FEMS Junior EUROMAT 2018, The Main Event for Young Materials Scientists, July 8-12, 2018/Budapest, Hungary},
   keywords = {graphene; sheets; carbon; microwave; torch discharge},
   language = {eng},
   isbn = {978-963-05-9917-7},
   title = {Synthesis and properties of free-standing graphene nanosheets at atmospheric pressure conditions},
   url = {https://static.akcongress.com/downloads/euromat/JuniorEuromat2018_Bookofabstracts.pdf},
   year = {2018}
}

TY  - CONF
ID  - 1597937
AU  - Toman, Jozef - Jašek, Ondřej - Jurmanová, Jana
PY  - 2018
TI  - Synthesis and properties of free-standing graphene nanosheets at atmospheric pressure conditions
SN  - 9789630599177
KW  - graphene
KW  - sheets
KW  - carbon
KW  - microwave
KW  - torch discharge
UR  - https://static.akcongress.com/downloads/euromat/JuniorEuromat2018_Bookofabstracts.pdf
N2  - Last decade two-dimensional carbon-based nanostructures such as graphene nanosheets, nanoribbons and carbon nanowalls have attracted much research interest, due to their remarkable properties combining high mechanical strength and flexibility, exceptional electronic and thermal conductivity, high carrier mobility and optical transparency. Potential application in different fields of science and technology include hydrogen and energy storage, reinforcement of polymer composites, electronics, electrochemical devices, or gas sensors. Our deposition process reported in this work is based on injecting ethanol vapours through a microwave plasma environment, where decomposition of ethanol molecules takes place. We used microwave plasma torch discharge (2.45 GHz, ~200 W, Figure 1) operating at atmospheric pressure conditions to synthesize graphene nanosheets with rectangular shape and typical size of hundreds of nanometres. Argon flowing through the central channel of the nozzle was used as the working gas to ignite the discharge. Mixture consisting of ethanol vapours and additional argon flow was delivered into plasma environment by outer channel of the nozzle. Wide range of deposition conditions resulted in synthesis of different types of carbon material. However, mastering the deposition process by setting specific set of deposition conditions led to synthesis of graphene sheets (Figure 2). Created samples were analysed by scanning electron microscopy, Raman spectroscopy and X-ray photoelectron spectroscopy to probe the morphological, chemical and microstructural features of the produced material.
ER  -

TOMAN, Jozef, Ondřej JAŠEK a Jana JURMANOVÁ. Synthesis and properties of free-standing graphene nanosheets at atmospheric pressure conditions. In \textit{FEMS Junior EUROMAT 2018, The Main Event for Young Materials Scientists, July 8-12, 2018/Budapest, Hungary}. 2018. ISBN~978-963-05-9917-7.

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