Dual imaging of uranium ore by Laser Ablation Inductively
Coupled Plasma Mass Spectrometry and Laser Induced Breakdown
Spectroscopy

J 2021

Dual imaging of uranium ore by Laser Ablation Inductively Coupled Plasma Mass Spectrometry and Laser Induced Breakdown Spectroscopy

HOLÁ, Markéta, Karel NOVOTNÝ, Jan DOBEŠ, Ivo KREMPL, Vojtěch WERTICH et. al.

Basic information

Original name

Dual imaging of uranium ore by Laser Ablation Inductively Coupled Plasma Mass Spectrometry and Laser Induced Breakdown Spectroscopy

Authors

HOLÁ, Markéta (203 Czech Republic, belonging to the institution), Karel NOVOTNÝ (203 Czech Republic, guarantor, belonging to the institution), Jan DOBEŠ (203 Czech Republic, belonging to the institution), Ivo KREMPL (203 Czech Republic, belonging to the institution), Vojtěch WERTICH (203 Czech Republic, belonging to the institution), Juraj MOZOLA (703 Slovakia, belonging to the institution), Martin KUBEŠ (203 Czech Republic, belonging to the institution), Veronika FALTUSOVÁ (703 Slovakia, belonging to the institution), Jaromír LEICHMANN (203 Czech Republic, belonging to the institution) and Viktor KANICKÝ (203 Czech Republic, belonging to the institution)

Edition

Spectrochimica Acta, Part B: Atomic Spectroscopy, Oxford, Pergamon-Elsevier Science Ltd, 2021, 0584-8547

Other information

Language

English

Type of outcome

Článek v odborném periodiku

Field of Study

10505 Geology

Country of publisher

United Kingdom of Great Britain and Northern Ireland

Confidentiality degree

není předmětem státního či obchodního tajemství

References:

URL

Impact factor

Impact factor: 3.662

RIV identification code

RIV/00216224:14310/21:00123045

Organization unit

Faculty of Science

DOI

http://dx.doi.org/10.1016/j.sab.2021.106312

UT WoS

000712264000001

Keywords in English

LA-ICP-MS; LIBS; Elemental imaging; Elemental mapping; Uranium ore; Geological samples

Abstract

V originále

The great potential in combining two elemental imaging techniques - Laser Induced Breakdown Spectroscopy (LIBS) and Laser Ablation Inductively Coupled Plasma Mass Spectrometry (LA-ICP-MS) is demonstrated for uranium ore sample investigation. Dual imaging provides the advantages of both methods - high speed, large area imaging and additional evaluation of the whole spectrum for LIBS, and high resolution, low detection limits and isotopic imaging for LA-ICP-MS. Special software, ILAPS, was created for data processing to ensure the consistency of the resulting element images and the possibility of their combination. This new method for merging LIBS and LA-ICP-MS imaging data allows the display of detailed structures on the background of the overall sample image. Information contained in the detailed structures together with an overall view of the sample was displayed in one image to visualise the complete data from both methods. The effectiveness and usefulness of this new approach were demonstrated in identifying the structures responsible for elements migration in the uranium ore sample.

Links

EF16_026/0008459, research and development project

Name: Dlouhodobý výzkum geochemických bariér pro ukládání jaderného odpadu

MUNI/A/1390/2020, interní kód MU

Name: Analytická a fyzikální chemie ve výzkumu biologických, geologických a syntetických materiálů (Acronym: BIOGEOSYNT)

Investor: Masaryk University

Citovat

HOLÁ, Markéta, Karel NOVOTNÝ, Jan DOBEŠ, Ivo KREMPL, Vojtěch WERTICH, Juraj MOZOLA, Martin KUBEŠ, Veronika FALTUSOVÁ, Jaromír LEICHMANN and Viktor KANICKÝ. Dual imaging of uranium ore by Laser Ablation Inductively Coupled Plasma Mass Spectrometry and Laser Induced Breakdown Spectroscopy. Spectrochimica Acta, Part B: Atomic Spectroscopy. Oxford: Pergamon-Elsevier Science Ltd, 2021, vol. 186, December, p. 106312-106322. ISSN 0584-8547. Available from: https://dx.doi.org/10.1016/j.sab.2021.106312.

@article{1806357,
   author = {Holá, Markéta and Novotný, Karel and Dobeš, Jan and Krempl, Ivo and Wertich, Vojtěch and Mozola, Juraj and Kubeš, Martin and Faltusová, Veronika and Leichmann, Jaromír and Kanický, Viktor},
   article_location = {Oxford},
   article_number = {December},
   doi = {http://dx.doi.org/10.1016/j.sab.2021.106312},
   keywords = {LA-ICP-MS; LIBS; Elemental imaging; Elemental mapping; Uranium ore; Geological samples},
   language = {eng},
   issn = {0584-8547},
   journal = {Spectrochimica Acta, Part B: Atomic Spectroscopy},
   title = {Dual imaging of uranium ore by Laser Ablation Inductively Coupled Plasma Mass Spectrometry and Laser Induced Breakdown Spectroscopy},
   url = {https://www.sciencedirect.com/science/article/pii/S058485472100269X},
   volume = {186},
   year = {2021}
}

TY  - JOUR
ID  - 1806357
AU  - Holá, Markéta - Novotný, Karel - Dobeš, Jan - Krempl, Ivo - Wertich, Vojtěch - Mozola, Juraj - Kubeš, Martin - Faltusová, Veronika - Leichmann, Jaromír - Kanický, Viktor
PY  - 2021
TI  - Dual imaging of uranium ore by Laser Ablation Inductively Coupled Plasma Mass Spectrometry and Laser Induced Breakdown Spectroscopy
JF  - Spectrochimica Acta, Part B: Atomic Spectroscopy
VL  - 186
IS  - December
SP  - 106312
EP  - 106312
PB  - Pergamon-Elsevier Science Ltd
SN  - 05848547
KW  - LA-ICP-MS
KW  - LIBS
KW  - Elemental imaging
KW  - Elemental mapping
KW  - Uranium ore
KW  - Geological samples
UR  - https://www.sciencedirect.com/science/article/pii/S058485472100269X
N2  - The great potential in combining two elemental imaging techniques - Laser Induced Breakdown Spectroscopy (LIBS) and Laser Ablation Inductively Coupled Plasma Mass Spectrometry (LA-ICP-MS) is demonstrated for uranium ore sample investigation. Dual imaging provides the advantages of both methods - high speed, large area imaging and additional evaluation of the whole spectrum for LIBS, and high resolution, low detection limits and isotopic imaging for LA-ICP-MS. Special software, ILAPS, was created for data processing to ensure the consistency of the resulting element images and the possibility of their combination. This new method for merging LIBS and LA-ICP-MS imaging data allows the display of detailed structures on the background of the overall sample image. Information contained in the detailed structures together with an overall view of the sample was displayed in one image to visualise the complete data from both methods. The effectiveness and usefulness of this new approach were demonstrated in identifying the structures responsible for elements migration in the uranium ore sample.
ER  -

HOLÁ, Markéta, Karel NOVOTNÝ, Jan DOBEŠ, Ivo KREMPL, Vojtěch WERTICH, Juraj MOZOLA, Martin KUBEŠ, Veronika FALTUSOVÁ, Jaromír LEICHMANN and Viktor KANICKÝ. Dual imaging of uranium ore by Laser Ablation Inductively Coupled Plasma Mass Spectrometry and Laser Induced Breakdown Spectroscopy. \textit{Spectrochimica Acta, Part B: Atomic Spectroscopy}. Oxford: Pergamon-Elsevier Science Ltd, 2021, vol.~186, December, p.~106312-106322. ISSN~0584-8547. Available from: https://dx.doi.org/10.1016/j.sab.2021.106312.

Detailed Information on Publication Record