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@article{197549,
author = {Kanický, Viktor and Mermet, Jean and Michel},
article_location = {Berlin},
article_number = {7/8},
keywords = {Inductively Coupled Plasma; Atomic Emission Spectrometry; Laser Ablation; Silicates; Lithiumtetraborate Fusion;},
language = {eng},
issn = {0937-0633},
journal = {Fresenius Journal of Analytical Chemistry},
note = {Project PECO No. ERB3510PL921006},
title = {Selection of internal standards for analysis of silicate rocks and limestones by laser ablation inductively coupled plasma atomic emission spectrometry},
volume = {355},
year = {1996}
}
TY - JOUR
ID - 197549
AU - Kanický, Viktor - Mermet, Jean - Michel
PY - 1996
TI - Selection of internal standards for analysis of silicate rocks and limestones by laser ablation inductively coupled plasma atomic emission spectrometry
JF - Fresenius Journal of Analytical Chemistry
VL - 355
IS - 7/8
SP - 887
EP - 887
PB - Springer-Verlag
SN - 09370633
N1 - Project PECO No. ERB3510PL921006
KW - Inductively Coupled Plasma
KW - Atomic Emission Spectrometry
KW - Laser Ablation
KW - Silicates
KW - Lithiumtetraborate Fusion;
N2 - Included (Si, Ca) and added (Li, B) internal standards (IS) have been used comparatively in LA-ICP AES of silicates and limestones to improve both precision and accuracy. A Q-switched Nd:YAG laser (355 nm, 10 Hz, 10 mJ per shot) has been applied for ablation, Samples have been prepared by fusion with Li2B4O7 and measured using a Perkin-Elmer Optima 3000 ICP system, Both types of IS have given a relative standard deviation (RSD) less than 2-1%, which improved the repeatability by a factor of 2-10 and calibration graphs have been linear over the whole concentration range.
ER -
KANICKÝ, Viktor a Jean - Michel MERMET. Selection of internal standards for analysis of silicate rocks and limestones by laser ablation inductively coupled plasma atomic emission spectrometry. \textit{Fresenius Journal of Analytical Chemistry}. Berlin: Springer-Verlag, 1996, roč.~355, 7/8, s.~887-888. ISSN~0937-0633.
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