Determination of Zr and Ti in 3-micrometers-thick ZrTiN ceramic coatings using laser ablation inductively coupled plasma atomic emission spectrometry

KANICKÝ, Viktor, Jan MUSIL a Jean - Michel MERMET. Determination of Zr and Ti in 3-micrometers-thick ZrTiN ceramic coatings using laser ablation inductively coupled plasma atomic emission spectrometry. Applied Spectroscopy. USA: Society Appl. Spectroscopy, 1997, roč. 51, č. 7, s. 1037-1041. ISSN 0003-7028.

Základní údaje

Originální název

Determination of Zr and Ti in 3-micrometers-thick ZrTiN ceramic coatings using laser ablation inductively coupled plasma atomic emission spectrometry

Autoři

KANICKÝ, Viktor (203 Česká republika, garant), Jan MUSIL (203 Česká republika) a Jean - Michel MERMET (250 Francie)

Vydání

Applied Spectroscopy, USA, Society Appl. Spectroscopy, 1997, 0003-7028

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Další údaje

Jazyk

angličtina

Typ výsledku

Článek v odborném periodiku

Obor

10406 Analytical chemistry

Stát vydavatele

Spojené státy

Utajení

není předmětem státního či obchodního tajemství

Impakt faktor

Impact factor: 1.848

Organizační jednotka

Přírodovědecká fakulta

Klíčová slova anglicky

Atomic emission spectrometry; inductively coupled plasma; UV laser ablation; Coating analysis; Nitride ceramic coatings

Štítky

atomic emission spectrometry, Coating analysis, inductively coupled plasma, Nitride ceramic coatings, UV laser ablation

Příznaky

Recenzováno

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Anotace

V originále

Analysis of 3-mu m-thick ZrN, TIN, and ZrTiN ceramic coatings on a high-speed steel substrate by laser ablation inductively coupled plasma atomic emission spectrometry (LA-ICP-AES) is described, A Nd:YAG laser was used in the Q-switched mode and operated at 355 nm and 5 mJ, Ablation patterns were obtained on the target surface by moving the ablation chamber with respect to the laser beam by means of an X-Y translator, Control of the depth of penetration was obtained by successively performing a limited number of cycles. Transient signals were obtained and their peak areas were used for the construction of calibration graphs based on the concentrations determined by energy-dispersive X-ray (EDX) analysis, An erosion rate of 0.1 mu m per cycle was observed, Crater shape and depth, temporal behavior, and reproducibility of the signals are described.

Česky

Analysis of 3-mu m-thick ZrN, TIN, and ZrTiN ceramic coatings on a high-speed steel substrate by laser ablation inductively coupled plasma atomic emission spectrometry (LA-ICP-AES) is described, A Nd:YAG laser was used in the Q-switched mode and operated at 355 nm and 5 mJ, Ablation patterns were obtained on the target surface by moving the ablation chamber with respect to the laser beam by means of an X-Y translator, Control of the depth of penetration was obtained by successively performing a limited number of cycles. Transient signals were obtained and their peak areas were used for the construction of calibration graphs based on the concentrations determined by energy-dispersive X-ray (EDX) analysis, An erosion rate of 0.1 mu m per cycle was observed, Crater shape and depth, temporal behavior, and reproducibility of the signals are described.