| JONAS, Vladimír, Anna TÝČOVÁ, Jan PŘIKRYL, Adéla KOTZIANOVÁ, Vladimír VELEBNÝ and František FORET. Nanospray-assisted deposition of silver nanoparticles for mapping of a peptide in nanofibrous layers via surface-enhanced Raman spectrometry. Talanta. Elsevier, 2023, vol. 256, May, p. 1-8. ISSN 0039-9140. Available from: https://dx.doi.org/10.1016/j.talanta.2023.124313. |
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@article{2251560,
author = {Jonas, Vladimír and Týčová, Anna and Přikryl, Jan and Kotzianová, Adéla and Velebný, Vladimír and Foret, František},
article_number = {May},
doi = {http://dx.doi.org/10.1016/j.talanta.2023.124313},
keywords = {Colloid; Nanofibers; Nanoparticles; Nanospray; Mapping; Surface-enhanced Raman spectrometry},
language = {eng},
issn = {0039-9140},
journal = {Talanta},
note = {Pre-Proof},
title = {Nanospray-assisted deposition of silver nanoparticles for mapping of a peptide in nanofibrous layers via surface-enhanced Raman spectrometry},
url = {https://doi.org/10.1016/j.talanta.2023.124313},
volume = {256},
year = {2023}
}
TY - JOUR
ID - 2251560
AU - Jonas, Vladimír - Týčová, Anna - Přikryl, Jan - Kotzianová, Adéla - Velebný, Vladimír - Foret, František
PY - 2023
TI - Nanospray-assisted deposition of silver nanoparticles for mapping of a peptide in nanofibrous layers via surface-enhanced Raman spectrometry
JF - Talanta
VL - 256
IS - May
SP - 1-8
EP - 1-8
PB - Elsevier
SN - 00399140
N1 - Pre-Proof
KW - Colloid
KW - Nanofibers
KW - Nanoparticles
KW - Nanospray
KW - Mapping
KW - Surface-enhanced Raman spectrometry
UR - https://doi.org/10.1016/j.talanta.2023.124313
N2 - Surface-enhanced Raman spectrometry (SERS) is a universal detection tool identifying molecules via vibrations of their chemical bonds. Its function requires the close localization of metal nanostructures and the analyte. In this work, we present a lab-made instrumentation for the deposition of silver nanoparticles on a strongly hydrophilic nanofibrous composite via a nanospray for SERS mapping of an incorporated peptide. The nanospray-sample distance was revealed as the most crucial parameter since it directly influences the moisture of the deposited colloid. Residual water was recognized as a sensitivity enhancer. Additionally, we continuously introduced a solution of sodium chloride to the colloid increasing its ionic strength, which formed a more homogeneous profile of the deposit. After the deposition process, the treated sample was scanned via a SERS laser and the collected Raman spectra were transformed into a distribution map of the peptide at a concentration of 5 μg/g.
ER -
JONAS, Vladimír, Anna TÝČOVÁ, Jan PŘIKRYL, Adéla KOTZIANOVÁ, Vladimír VELEBNÝ and František FORET. Nanospray-assisted deposition of silver nanoparticles for mapping of a peptide in nanofibrous layers via surface-enhanced Raman spectrometry. \textit{Talanta}. Elsevier, 2023, vol.~256, May, p.~1-8. ISSN~0039-9140. Available from: https://dx.doi.org/10.1016/j.talanta.2023.124313.
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