| MALOVANÁ, Sabina, F.J. GARCÍA MONTELONGO, J.P. PÉREZ a M.A. RODRÍGUREZ-DELGADO. Optimisation of sample preparation for the determination of trans-resveratrol and other polyphenolic compounds in wines by high performance liquid chromatography. Analytica Chimica Acta. 2001, č. 428, s. 245-253. ISSN 0003-2670. |
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@article{366775,
author = {Malovaná, Sabina and García Montelongo, F.J. and Pérez, J.P. and RodrígurezandDelgado, M.A.},
article_number = {428},
keywords = {trans-Resveratrol; Phenolic compounds; HPLC; Wine samples},
issn = {0003-2670},
journal = {Analytica Chimica Acta},
title = {Optimisation of sample preparation for the determination of trans-resveratrol and other polyphenolic compounds in wines by high performance liquid chromatography},
year = {2001}
}
TY - JOUR
ID - 366775
AU - Malovaná, Sabina - García Montelongo, F.J. - Pérez, J.P. - Rodrígurez-Delgado, M.A.
PY - 2001
TI - Optimisation of sample preparation for the determination of trans-resveratrol and other polyphenolic compounds in wines by high performance liquid chromatography
JF - Analytica Chimica Acta
IS - 428
SP - 245
EP - 245
SN - 00032670
KW - trans-Resveratrol
KW - Phenolic compounds
KW - HPLC
KW - Wine samples
N2 - Different methods for sample preparation as a preliminary stage for the simultaneous determination of trans-resveratrol and other polyphenolic compounds are compared with the aim to establish the best conditions for the determination of these compounds in wine samples by high performance liquid chromatography (HPLC). Sample preparation using liquid-liquid extraction and solid-phase extraction were compared. Liquid-liquid extraction using as organic solvent diethyl ether at pH 2.0 shows the best results. The dried extract was solved in methanol/water 1:1 (v/v) that improve drastically the separation efficiency. The developed method was applied to the analysis of wines from the Canary Islands.
ER -
MALOVANÁ, Sabina, F.J. GARCÍA MONTELONGO, J.P. PÉREZ a M.A. RODRÍGUREZ-DELGADO. Optimisation of sample preparation for the determination of trans-resveratrol and other polyphenolic compounds in wines by high performance liquid chromatography. \textit{Analytica Chimica Acta}. 2001, č.~428, s.~245-253. ISSN~0003-2670.
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