Detailed Information on Publication Record
2009
Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry
ŠVÁBENSKÝ, Radim, Michal ORAVEC and Zdeněk ŠIMEKBasic information
Original name
Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry
Name in Czech
Stanovení polycyklických aromatických dusíkatých heterocyklů pomocí kapalinové chromatografie s tandemovou hmotnostní detekcí.
Authors
ŠVÁBENSKÝ, Radim (203 Czech Republic), Michal ORAVEC (203 Czech Republic) and Zdeněk ŠIMEK (203 Czech Republic, guarantor)
Edition
International Journal of Environmental analytical cemistry, 2009, 0306-7319
Other information
Language
English
Type of outcome
Článek v odborném periodiku
Field of Study
10406 Analytical chemistry
Country of publisher
United Kingdom of Great Britain and Northern Ireland
Confidentiality degree
není předmětem státního či obchodního tajemství
Impact factor
Impact factor: 1.703
RIV identification code
RIV/00216224:14310/09:00036101
Organization unit
Faculty of Science
UT WoS
000263288600003
Keywords in English
polycyclic aromatic nitrogen heterocycles; PANHs; soil; LC-ESI/MS/MS
Tags
International impact, Reviewed
Změněno: 8/3/2010 22:43, doc. RNDr. Zdeněk Šimek, CSc.
V originále
Development of LC/MS/MS method for analysing polycyclic aromatic nitrogen hydrocarbons (PANHs) in soil samples is presented. Optimisation of individual chromatographic/mass spectrometric conditions was made in order to obtain a method for the determination of 15 PANHs content in an organic extract from the soil. Detection limits (LOD) in the range of 0.3 to 15 pg per injection were 15 obtained for individual PANHs. LC/MS/MS method has a lower LOD value compared to LC/DAD/FLD methods in general. Developed LC/MS/MS method was used for determination of PANHs content in soil samples collected in contaminated areas of the southeast region of the Czech Republic. Highest concentrations of PANHs have been found in the samples collected in the immediate vicinity of the industrial basin. Concentrations of the contaminants in samples collected in surrounding villages were higher compared to the sample collected in clean area of the Czech Republic.
In Czech
Development of LC/MS/MS method for analysing polycyclic aromatic nitrogen hydrocarbons (PANHs) in soil samples is presented. Optimisation of individual chromatographic/mass spectrometric conditions was made in order to obtain a method for the determination of 15 PANHs content in an organic extract from the soil. Detection limits (LOD) in the range of 0.3 to 15 pg per injection were 15 obtained for individual PANHs. LC/MS/MS method has a lower LOD value compared to LC/DAD/FLD methods in general. Developed LC/MS/MS method was used for determination of PANHs content in soil samples collected in contaminated areas of the southeast region of the Czech Republic. Highest concentrations of PANHs have been found in the samples collected in the immediate vicinity of the industrial basin. Concentrations of the contaminants in samples collected in surrounding villages were higher compared to the sample collected in clean area of the Czech Republic.
Links
| MSM0021622412, plan (intention) |
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