C8870 Synthesis and analysis of new materials

Faculty of Science
Spring 2007
Extent and Intensity
0/5/0. 5 credit(s) (fasci plus compl plus > 4). Recommended Type of Completion: graded credit. Other types of completion: z (credit).
Teacher(s)
doc. RNDr. Pavel Brož, Ph.D. (seminar tutor)
doc. RNDr. Zdeněk Losos, CSc. (seminar tutor)
prof. RNDr. Jiří Pinkas, Ph.D. (seminar tutor)
prof. RNDr. Jiří Sopoušek, CSc. (seminar tutor)
RNDr. Václav Vávra, Ph.D. (seminar tutor)
prof. RNDr. Jan Vřešťál, DrSc. (seminar tutor)
Guaranteed by
prof. RNDr. Jiří Pinkas, Ph.D.
Department of Chemistry – Chemistry Section – Faculty of Science
Contact Person: prof. RNDr. Jiří Pinkas, Ph.D.
Prerequisites
C7780 Inorganic Materials Chemistry
Knowledge level of the basic courses of general, inorganic, physical, and analytical chemistry.
Course Enrolment Limitations
The course is offered to students of any study field.
Course objectives
The course give the basic overview of the most important synthetic methods currently used for the synthesis of metallic and nonmetallic inorganic materials. High-temperature solid state reactions, solid-gas reactions, coprecipitation method, hydrothermal synthesis, supramolecular templating, and sonochemical method are introduced. Furthermore, basic characterization techniques are applied to the prepared samples, such as X-ray powder diffraction, analysis of the specific surface area by the BET method, thermal analysis, solid state NMR spectroscopy, optical and scanning electron microscopy, and testing of mechanical properties of solids.
Syllabus
  • List of experiments for C8870 Synthesis and analysis of materials

    1. Synthesis of the YBCO superconductor.

    2. Synthesis of zeolite X.

    3. Synthesis of mesoporous MCM-41 materials.

    4. Preparation of binary Pb/Sn alloys and construction of the phase diagram.

    5. Synthesis of nanoscopic Fe2O3 by sonochemical method.

    6. Thermochemical treatment of metallic materials.

    7. Analysis of the specific surface area by the BET method.

    8. Thermal analysis.

    9. Scanning electron microscopy.

    10. X-ray powder diffraction.

    11. Optical microscopy, refractive index.

    12. Mechanical properties of solids.

    13. Solid state NMR spectroscopy.
Literature
  • Literatura uvedena u jednotlivých úloh
Assessment methods (in Czech)
Před absolvováním každé úlohy bude provedena zkouška znalostí teoretického základu a postupu práce. Z každé úlohy bude vypracován protokol podle pokynů uvedených u úlohy. Závěrečný test bude obsahovat otázky k principům všech úloh.
Language of instruction
Czech
Further comments (probably available only in Czech)
The course is taught annually.
The course is taught: every week.
Teacher's information
http://sci.muni.cz/chemsekce/c8870/
The course is also listed under the following terms Spring 2008 - for the purpose of the accreditation, Spring 2011 - only for the accreditation, Spring 2000, Spring 2001, Spring 2002, Spring 2005, Spring 2006, Spring 2008, Spring 2009, Spring 2010, Spring 2011, Spring 2012, spring 2012 - acreditation, Spring 2013, Spring 2014, Spring 2015, Spring 2016, Spring 2017, spring 2018, Spring 2019, Spring 2020, Spring 2021, Spring 2022, Spring 2023, Spring 2024, Spring 2025.
  • Enrolment Statistics (Spring 2007, recent)
  • Permalink: https://is.muni.cz/course/sci/spring2007/C8870