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@article{1068870,
author = {Spíchal, Zdeněk and Pinkas, Jiří and Nečas, Marek},
article_number = {1},
doi = {http://dx.doi.org/10.1016/j.poly.2012.08.056},
keywords = {Diphenylphosphorylvaleric acid; Praseodymium; Coordination polymers; X-ray crystallography},
language = {eng},
issn = {0277-5387},
journal = {Polyhedron},
title = {Solvent-induced changes in dimensionality of praseodymium coordination polymers with diphenylphosphorylvalerate ligand},
url = {http://dx.doi.org/10.1016/j.poly.2012.08.056},
volume = {48},
year = {2012}
}
TY - JOUR
ID - 1068870
AU - Spíchal, Zdeněk - Pinkas, Jiří - Nečas, Marek
PY - 2012
TI - Solvent-induced changes in dimensionality of praseodymium coordination polymers with diphenylphosphorylvalerate ligand
JF - Polyhedron
VL - 48
IS - 1
SP - 99-103
EP - 99-103
PB - Elsevier Science Ltd.
SN - 02775387
KW - Diphenylphosphorylvaleric acid
KW - Praseodymium
KW - Coordination polymers
KW - X-ray crystallography
UR - http://dx.doi.org/10.1016/j.poly.2012.08.056
L2 - http://dx.doi.org/10.1016/j.poly.2012.08.056
N2 - Architectures of coordination polymers resulting from the reaction of diphenylphosphorylvaleric acid (1) with Pr(NO3)3.6H2O in the presence of a base can be controlled by the solvent. While in methanolic solution a two-dimensional network Pr2(1–H)3(NO3)3 (1m) with a 1:1.5 metal-to-ligand ratio was formed, the aqueous media induced the formation of a three-dimensional framework Pr(1–H)2(NO3) (1w) with a 1:2 metal-to-ligand ratio. The compounds were studied by single crystal X-ray diffraction, IR spectroscopy, ESI-TOF mass spectrometry, and thermal analysis TG/DSC techniques.
ER -
SPÍCHAL, Zdeněk, Jiří PINKAS a Marek NEČAS. Solvent-induced changes in dimensionality of praseodymium coordination polymers with diphenylphosphorylvalerate ligand. \textit{Polyhedron}. Elsevier Science Ltd., roč.~48, č.~1, s.~99-103. ISSN~0277-5387. doi:10.1016/j.poly.2012.08.056. 2012.
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