Estimating the degree of Mg corrosion using laser-induced
breakdown spectroscopy

a 2015

Estimating the degree of Mg corrosion using laser-induced breakdown spectroscopy

POŘÍZKA, Pavel; Ivana ROČŇÁKOVÁ; Lucia SLÁDKOVÁ; Jakub KLUS; David PROCHAZKA et al.

Základní údaje

Originální název

Estimating the degree of Mg corrosion using laser-induced breakdown spectroscopy

Autoři

POŘÍZKA, Pavel; Ivana ROČŇÁKOVÁ; Lucia SLÁDKOVÁ; Jakub KLUS; David PROCHAZKA; Jan NOVOTNÝ; Karel NOVOTNÝ a Jozef KAISER

Vydání

European Winter Conference on Plasma Spectrochemistry 2015, 2015

Další údaje

Jazyk

angličtina

Typ výsledku

Konferenční abstrakt

Obor

10406 Analytical chemistry

Stát vydavatele

Německo

Utajení

není předmětem státního či obchodního tajemství

Odkazy

URL

Označené pro přenos do RIV

Ano

Kód RIV

RIV/00216224:14740/15:00086575

Organizační jednotka

Středoevropský technologický institut

Klíčová slova anglicky

estimation of corrosion degree; LIBS

Změněno: 15. 2. 2016 17:10, doc. Mgr. Karel Novotný, Ph.D.

Anotace

V originále

We report on the potential use of laser-induced breakdown spectroscopy (LIBS) for direct estimation of Mg corrosion degree. This work concerns optimization and comparison of the table-top and stand-off LIBS systems as well as the preliminary study to prove the capability of LIBS technique for corrosion detection. In order to simulate real corrosive environment, Mg samples were prepared in the aging chamber. The properties of corrosive layer on the surface of the sample significantly affect the laser-matter interaction, i.e. the matrix effect. Consequently, the properties and persistence of laser-induced plasmas (LIPs), generated on such degraded surfaces, essentially differ. Collected radiation of LIPs is then analysed and the intensities of ionic and/or atomic spectral lines are correlated with the degree of metallic corrosion. Parallelly, X-ray computed microtomography (uCT), metallographic tests and optical profilometry were utilized to obtain more complex information about the degraded samples. The research is focused on demonstrating the utilization of LIBS as an method available for fast evaluation of the corrosion of metallic surfaces. Furthermore, this analysis may be beneficially performed by means of LIBS in real-time and even in-situ using remote or stand-off variations of LIBS device. Moreover, the bottom line of this research is the application of stand-off LIBS technique in civil engineering.

Návaznosti

ED1.1.00/02.0068, projekt VaV

Název: CEITEC - central european institute of technology

Citovat

POŘÍZKA, Pavel; Ivana ROČŇÁKOVÁ; Lucia SLÁDKOVÁ; Jakub KLUS; David PROCHAZKA; Jan NOVOTNÝ; Karel NOVOTNÝ a Jozef KAISER. Estimating the degree of Mg corrosion using laser-induced breakdown spectroscopy. In European Winter Conference on Plasma Spectrochemistry 2015. 2015.

@proceedings{1335284,
   author = {Pořízka, Pavel and Ročňáková, Ivana and Sládková, Lucia and Klus, Jakub and Prochazka, David and Novotný, Jan and Novotný, Karel and Kaiser, Jozef},
   booktitle = {European Winter Conference on Plasma Spectrochemistry 2015},
   keywords = {estimation of corrosion degree; LIBS},
   language = {eng},
   title = {Estimating the degree of Mg corrosion using laser-induced breakdown spectroscopy},
   url = {http://www.ewcps2015.org/program/show.html?aid=499&pid=253&bck=/program/day-3/session-1},
   year = {2015}
}

TY  - CONF
ID  - 1335284
AU  - Pořízka, Pavel - Ročňáková, Ivana - Sládková, Lucia - Klus, Jakub - Prochazka, David - Novotný, Jan - Novotný, Karel - Kaiser, Jozef
PY  - 2015
TI  - Estimating the degree of Mg corrosion using laser-induced breakdown spectroscopy
KW  - estimation of corrosion degree
KW  - LIBS
UR  - http://www.ewcps2015.org/program/show.html?aid=499&pid=253&bck=/program/day-3/session-1
N2  - We report on the potential use of laser-induced breakdown spectroscopy (LIBS) for direct estimation of Mg corrosion degree. This work concerns optimization and comparison of the table-top and stand-off LIBS systems as well as the preliminary study to prove the capability of LIBS technique for corrosion detection. In order to simulate real corrosive environment, Mg samples were prepared in the aging chamber. The properties of corrosive layer on the surface of the sample significantly affect the laser-matter interaction, i.e. the matrix effect. Consequently, the properties and persistence of laser-induced plasmas (LIPs), generated on such degraded surfaces, essentially differ. Collected radiation of LIPs is then analysed and the intensities of ionic and/or atomic spectral lines are correlated with the degree of metallic corrosion. Parallelly, X-ray computed microtomography (uCT), metallographic tests and optical profilometry were utilized to obtain more complex information about the degraded samples. The research is focused on demonstrating the utilization of LIBS as an method available for fast evaluation of the corrosion of metallic surfaces. Furthermore, this analysis may be beneficially performed by means of LIBS in real-time and even in-situ using remote or stand-off variations of LIBS device. Moreover, the bottom line of this research is the application of stand-off LIBS technique in civil engineering.
ER  -

POŘÍZKA, Pavel; Ivana ROČŇÁKOVÁ; Lucia SLÁDKOVÁ; Jakub KLUS; David PROCHAZKA; Jan NOVOTNÝ; Karel NOVOTNÝ a Jozef KAISER. Estimating the degree of Mg corrosion using laser-induced breakdown spectroscopy. In \textit{European Winter Conference on Plasma Spectrochemistry 2015}. 2015.

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