| MEDVECKÁ, Veronika, Dušan KOVÁČIK, Anna ZAHORANOVÁ a Mirko ČERNÁK. Atmospheric pressure plasma assisted calcination by the preparation of TiO2 fibers in submicron scale. Applied Surface Science. AMSTERDAM: North-Holland, 2018, roč. 428, January, s. 609-615. ISSN 0169-4332. Dostupné z: https://dx.doi.org/10.1016/j.apsusc.2017.09.178. |
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@article{1406908,
author = {Medvecká, Veronika and Kováčik, Dušan and Zahoranová, Anna and Černák, Mirko},
article_location = {AMSTERDAM},
article_number = {January},
doi = {http://dx.doi.org/10.1016/j.apsusc.2017.09.178},
keywords = {Inorganic fibers; Plasma assisted calcination; Atmospheric pressure plasma; Dielectric barrier discharges; Coplanar discharge},
language = {eng},
issn = {0169-4332},
journal = {Applied Surface Science},
title = {Atmospheric pressure plasma assisted calcination by the preparation of TiO2 fibers in submicron scale},
url = {https://www.sciencedirect.com/science/article/pii/S016943321732826X},
volume = {428},
year = {2018}
}
TY - JOUR
ID - 1406908
AU - Medvecká, Veronika - Kováčik, Dušan - Zahoranová, Anna - Černák, Mirko
PY - 2018
TI - Atmospheric pressure plasma assisted calcination by the preparation of TiO2 fibers in submicron scale
JF - Applied Surface Science
VL - 428
IS - January
SP - 609-615
EP - 609-615
PB - North-Holland
SN - 01694332
KW - Inorganic fibers
KW - Plasma assisted calcination
KW - Atmospheric pressure plasma
KW - Dielectric barrier discharges
KW - Coplanar discharge
UR - https://www.sciencedirect.com/science/article/pii/S016943321732826X
L2 - https://www.sciencedirect.com/science/article/pii/S016943321732826X
N2 - Atmospheric pressure plasma assisted calcination by the preparation of TiO2 submicron fibers as a low-temperature alternative to the conventional thermal annealing was studied. A special type of dielectric barrier discharge was used for plasma treatment of hybrid titanium butoxide/polyvinylpyrrolidone (Ti(Bu)/PVP) fibers prepared by forcespinning to decompose and oxidize the base polymer and precursor. The obtained fibers were characterized by changes in chemical bonds on the surface using Fourier Transform Infrared Spectroscopy (FTIR), chemical composition by using Energy-Dispersive X-Ray Spectroscopy (EDX), X-ray Photoelectron Spectroscopy (XPS). The morphology of fibers was investigated by Scanning Electron Microscopy (SEM). A significant decrease of organic components was reached by short plasma exposure times less than 1 h. The obtained fibers exhibit a high surface porosity without degradation of the fibrous structure. The results obtained indicate that atmospheric pressure plasma assisted calcination can be a viable low-temperature, energy-and time-saving alternative or pre-treatment method for the conventional high-temperature thermal calcination.
ER -
MEDVECKÁ, Veronika, Dušan KOVÁČIK, Anna ZAHORANOVÁ a Mirko ČERNÁK. Atmospheric pressure plasma assisted calcination by the preparation of TiO2 fibers in submicron scale. \textit{Applied Surface Science}. AMSTERDAM: North-Holland, 2018, roč.~428, January, s.~609-615. ISSN~0169-4332. Dostupné z: https://dx.doi.org/10.1016/j.apsusc.2017.09.178.
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