ROZSYPAL, Jan, Daniel RIMAN, Vladimír HALOUZKA, Tomáš OPLETAL, David JIROVSKÝ, Mamas PRODROMIDIS a Jan HRBÁČ. Use of interelectrode material transfer of nickel and copper-nickel alloy to carbon fibers to assemble miniature glucose sensors. Journal of Electroanalytical Chemistry. Lausanne: Elsevier, 2018, roč. 816, May 1, s. 45-53. ISSN 1572-6657. Dostupné z: https://dx.doi.org/10.1016/j.jelechem.2018.03.039. |
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@article{1412747, author = {Rozsypal, Jan and Riman, Daniel and Halouzka, Vladimír and Opletal, Tomáš and Jirovský, David and Prodromidis, Mamas and Hrbáč, Jan}, article_location = {Lausanne}, article_number = {May 1}, doi = {http://dx.doi.org/10.1016/j.jelechem.2018.03.039}, keywords = {Non enzymatic glucose sensor Anodic dissolution Nickel nanoparticles; Copper nickel alloyed nanoparticles; Carbon fiber microelectrode}, language = {eng}, issn = {1572-6657}, journal = {Journal of Electroanalytical Chemistry}, title = {Use of interelectrode material transfer of nickel and copper-nickel alloy to carbon fibers to assemble miniature glucose sensors}, url = {http://dx.doi.org/10.1016/j.jelechem.2018.03.039}, volume = {816}, year = {2018} }
TY - JOUR ID - 1412747 AU - Rozsypal, Jan - Riman, Daniel - Halouzka, Vladimír - Opletal, Tomáš - Jirovský, David - Prodromidis, Mamas - Hrbáč, Jan PY - 2018 TI - Use of interelectrode material transfer of nickel and copper-nickel alloy to carbon fibers to assemble miniature glucose sensors JF - Journal of Electroanalytical Chemistry VL - 816 IS - May 1 SP - 45-53 EP - 45-53 PB - Elsevier SN - 15726657 KW - Non enzymatic glucose sensor Anodic dissolution Nickel nanoparticles KW - Copper nickel alloyed nanoparticles KW - Carbon fiber microelectrode UR - http://dx.doi.org/10.1016/j.jelechem.2018.03.039 N2 - Electrochemical deposition of the material released by anodizing nickel and copper nickel alloy in pure water onto carbon fiber microelectrodes was used to assemble miniature glucose sensors. The composition and morphology of the deposits was investigated by scanning electron microscopy, energy dispersive X-ray spectroscopy and X-ray photoelectron spectroscopy. The deposition of anode-derived materials proceeded by two consecutive mechanisms, which are explained in detail. The electrochemical properties of the designed electrodes were subsequently investigated by cyclic voltammetry and electrochemical impedance spectroscopy. The different Ni- and mixed CuNi-modified microelectrodes were examined as glucose sensors and the best performing electrodes based on the alloyed deposit exhibited very high sensitivity (5720 uA mM-1 cm-2), low detection limit (0.3 uM) and ability to quantify glucose in blood serum. ER -
ROZSYPAL, Jan, Daniel RIMAN, Vladimír HALOUZKA, Tomáš OPLETAL, David JIROVSKÝ, Mamas PRODROMIDIS a Jan HRBÁČ. Use of interelectrode material transfer of nickel and copper-nickel alloy to carbon fibers to assemble miniature glucose sensors. \textit{Journal of Electroanalytical Chemistry}. Lausanne: Elsevier, 2018, roč.~816, May 1, s.~45-53. ISSN~1572-6657. Dostupné z: https://dx.doi.org/10.1016/j.jelechem.2018.03.039.
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