HURLEY, Rachel R., Amy L. LUSHER, Marianne OLSEN a Luca NIZZETTO. Validation of a Method for Extracting Microplastics from Complex, Organic-Rich, Environmental Matrices. ENVIRONMENTAL SCIENCE & TECHNOLOGY. WASHINGTON: AMER CHEMICAL SOC, 2018, roč. 52, č. 13, s. 7409-7417. ISSN 0013-936X. Dostupné z: https://dx.doi.org/10.1021/acs.est.8b01517. |
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@article{1495619, author = {Hurley, Rachel R. and Lusher, Amy L. and Olsen, Marianne and Nizzetto, Luca}, article_location = {WASHINGTON}, article_number = {13}, doi = {http://dx.doi.org/10.1021/acs.est.8b01517}, keywords = {WATER TREATMENT PLANTS; WASTE-WATER; HYDROGEN-PEROXIDE; FENTONS REAGENT; SEWAGE-SLUDGE; MARINE-SEDIMENTS; SYNTHETIC-FIBERS; GREAT-LAKES; OXIDATION; FISH}, language = {eng}, issn = {0013-936X}, journal = {ENVIRONMENTAL SCIENCE & TECHNOLOGY}, title = {Validation of a Method for Extracting Microplastics from Complex, Organic-Rich, Environmental Matrices}, url = {https://pubs.acs.org/doi/10.1021/acs.est.8b01517}, volume = {52}, year = {2018} }
TY - JOUR ID - 1495619 AU - Hurley, Rachel R. - Lusher, Amy L. - Olsen, Marianne - Nizzetto, Luca PY - 2018 TI - Validation of a Method for Extracting Microplastics from Complex, Organic-Rich, Environmental Matrices JF - ENVIRONMENTAL SCIENCE & TECHNOLOGY VL - 52 IS - 13 SP - 7409-7417 EP - 7409-7417 PB - AMER CHEMICAL SOC SN - 0013936X KW - WATER TREATMENT PLANTS KW - WASTE-WATER KW - HYDROGEN-PEROXIDE KW - FENTONS REAGENT KW - SEWAGE-SLUDGE KW - MARINE-SEDIMENTS KW - SYNTHETIC-FIBERS KW - GREAT-LAKES KW - OXIDATION KW - FISH UR - https://pubs.acs.org/doi/10.1021/acs.est.8b01517 L2 - https://pubs.acs.org/doi/10.1021/acs.est.8b01517 N2 - Complex and organic-rich solid substrates such as sludge and soil have been shown to be contaminated by microplastics; however, methods for extracting plastic particles have not yet been systemically tested or standardized. This study investigated four main protocols for the removal of organic material during analysis of microplastics from complex solid matrices: oxidation using H2O2, Fenton's reagent, and alkaline digestion with NaOH and KOH. Eight common polymer types were used to assess the influence of reagent exposure on particle integrity. Organic matter removal efficiencies were established for test sludge and soil samples. Fenton's reagent was identified as the optimum protocol. All other methods showed signs of particle degradation or resulted in an insufficient reduction in organic matter content. A further validation procedure revealed high microplastic extraction efficiencies for particles with different morphologies. This confirmed the suitability of Fenton's reagent for use in conjunction with density separation for extracting microplastics. This approach affords greater comparability with existing studies that utilize a density-based technique. Recommendations for further method optimization were also identified to improve the recovery of microplastic from complex, organic-rich environmental samples. ER -
HURLEY, Rachel R., Amy L. LUSHER, Marianne OLSEN a Luca NIZZETTO. Validation of a Method for Extracting Microplastics from Complex, Organic-Rich, Environmental Matrices. \textit{ENVIRONMENTAL SCIENCE \&{}amp; TECHNOLOGY}. WASHINGTON: AMER CHEMICAL SOC, 2018, roč.~52, č.~13, s.~7409-7417. ISSN~0013-936X. Dostupné z: https://dx.doi.org/10.1021/acs.est.8b01517.
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