2019
Characterization of novel graphene-like materials prepared by new cheap and environmentally friendly synthetic methods
NĚMEČKOVÁ, Dana; richard ŠEVČÍK a Pavel PAZDERAZákladní údaje
Originální název
Characterization of novel graphene-like materials prepared by new cheap and environmentally friendly synthetic methods
Autoři
NĚMEČKOVÁ, Dana; richard ŠEVČÍK a Pavel PAZDERA
Vydání
The 23rd International Electronic Conference on Synthetic Organic Chemistry, 2019
Další údaje
Jazyk
angličtina
Typ výsledku
Prezentace na konferencích
Obor
10401 Organic chemistry
Stát vydavatele
Švýcarsko
Utajení
není předmětem státního či obchodního tajemství
Odkazy
Organizační jednotka
Přírodovědecká fakulta
Klíčová slova anglicky
graphene; graphene oxide; synthesis; characterization; green chemistry; sustainable chemistry, spectroscopy, ultrasound
Změněno: 25. 4. 2020 08:40, doc. RNDr. Pavel Pazdera, CSc.
Anotace
V originále
We report characterization data of novel graphene-like materials prepared by new cheap and environmentally friendly synthetic methods. FT-IR, Raman and X-ray photoelectron spectroscopy, scanning electron microscopy and thermal and elemental analysis methods were used to describe features of novel graphene-like materials and obtained data were compared with the data of commercial standards. It was found that employment of gentle oxidizing agents supported by ultrasound action instead of harsh oxidizers and strongly acidic solutions provides a-few-layer graphene oxides with low-defect layers in high yields. Although keeping the same level of oxidation like commercial standards new products are more stable due to a lower damage of carbon layers. Obtained products can then be further modified to reduced graphene oxides or amine-modified derivatives. All of the characterization data are presented and discussed in the article.