POURAYOUBI, Mehrdad, Monireh NEGARI a Marek NEČAS. N-Cyclohexylcyclohexanaminium chloride. Acta Crystallographica Section E: Structure Reports Online. Chester, UK: IUCr, 2011, roč. 67, FEB 2011, s. "O332"-"U321", 7 s. ISSN 1600-5368. Dostupné z: https://dx.doi.org/10.1107/S1600536811000857. |
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@article{1669709, author = {Pourayoubi, Mehrdad and Negari, Monireh and Nečas, Marek}, article_location = {Chester, UK}, article_number = {FEB 2011}, doi = {http://dx.doi.org/10.1107/S1600536811000857}, keywords = {single-crystal X-ray study; T = 120 K; mean (C–C) = 0.003 angstrom; R factor = 0.025; wR factor = 0.057; data-to-parameter ratio = 9.0}, language = {eng}, issn = {1600-5368}, journal = {Acta Crystallographica Section E: Structure Reports Online}, title = {N-Cyclohexylcyclohexanaminium chloride}, url = {https://doi.org/10.1107/S1600536811000857}, volume = {67}, year = {2011} }
TY - JOUR ID - 1669709 AU - Pourayoubi, Mehrdad - Negari, Monireh - Nečas, Marek PY - 2011 TI - N-Cyclohexylcyclohexanaminium chloride JF - Acta Crystallographica Section E: Structure Reports Online VL - 67 IS - FEB 2011 SP - "O332"-"U321" EP - "O332"-"U321" PB - IUCr SN - 16005368 KW - single-crystal X-ray study KW - T = 120 K KW - mean (C–C) = 0.003 angstrom KW - R factor = 0.025 KW - wR factor = 0.057 KW - data-to-parameter ratio = 9.0 UR - https://doi.org/10.1107/S1600536811000857 L2 - https://doi.org/10.1107/S1600536811000857 N2 - In the title salt, C12H24N+center dot Cl-, both cyclohexyl rings adopt chair conformations and the NH2 unit is situated in the equatorial position with respect to the rings in the cation. The large C-N-C bond angle [117.99 (14)degrees] in the cation is a result of linking two bulky cyclohexyl rings to the N atom. The aminium H atoms are involved in intermolecular N-H center dot center dot center dot Cl hydrogen bonds, forming an infinite zigzag chain parallel to the c axis. The crystal studied was a racemic twin with a twin fraction of 0.28 18). ER -
POURAYOUBI, Mehrdad, Monireh NEGARI a Marek NEČAS. N-Cyclohexylcyclohexanaminium chloride. \textit{Acta Crystallographica Section E: Structure Reports Online}. Chester, UK: IUCr, 2011, roč.~67, FEB 2011, s.~''O332''-''U321'', 7 s. ISSN~1600-5368. Dostupné z: https://dx.doi.org/10.1107/S1600536811000857.
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