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@article{203252,
author = {Pinkas, Jiří and Wessel, H. and Yang, Y. and Montero, M. L. and Noltemeyer, M. and Fröba, M. and Roesky, Herbert W.},
article_location = {Spojené státy americké},
article_number = {10},
keywords = {aluminum; gallium; phosphates; nonaqueous},
language = {eng},
issn = {0020-1669},
journal = {Inorg. Chem.},
title = {Reactions of Phosphoric Acid Triesters with Aluminium and Gallium Amides.},
volume = {37},
year = {1998}
}
TY - JOUR
ID - 203252
AU - Pinkas, Jiří - Wessel, H. - Yang, Y. - Montero, M. L. - Noltemeyer, M. - Fröba, M. - Roesky, Herbert W.
PY - 1998
TI - Reactions of Phosphoric Acid Triesters with Aluminium and Gallium Amides.
JF - Inorg. Chem.
VL - 37
IS - 10
SP - 2450
EP - 2450
PB - American Chemical Society
SN - 00201669
KW - aluminum
KW - gallium
KW - phosphates
KW - nonaqueous
N2 - AlPO4 and GaPO4 are formed in the reaction of phosphoric acid triesters OP(OR)3, (R = Me, Et, n-Bu, SiMe3) with aluminium and gallium amides [M(NMe2)3]2, M = Al (1), Ga (2), respectively, in nonaqueous solvents. The model for the initial step in these reactions is an adduct (Me2N)3Al.OPPh3 (3). AlPO4 also results from the reaction of AlCl3 with OP(OSiMe3)3. Alumazene gives a bis-adduct [MeAlNDipp]3.2OP(OMe)3 (5) with trimethyl phosphate.
ER -
PINKAS, Jiří, H. WESSEL, Y. YANG, M. L. MONTERO, M. NOLTEMEYER, M. FRÖBA a Herbert W. ROESKY. Reactions of Phosphoric Acid Triesters with Aluminium and Gallium Amides. \textit{Inorg. Chem.}. Spojené státy americké: American Chemical Society, 1998, roč.~37, č.~10, s.~2450-2457. ISSN~0020-1669.
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