Study of spectral lines behaviour with a double pulse 1064–1064
nm laser-induced breakdown spectroscopy system at the direct
analysis of algae on the filter

J 2024

Study of spectral lines behaviour with a double pulse 1064–1064 nm laser-induced breakdown spectroscopy system at the direct analysis of algae on the filter

HORSKÁ, Jana; Aleš HRDLIČKA; Jitka HEGROVÁ; Martina BUCKOVÁ; David PROCHAZKA et al.

Základní údaje

Originální název

Study of spectral lines behaviour with a double pulse 1064–1064 nm laser-induced breakdown spectroscopy system at the direct analysis of algae on the filter

Autoři

HORSKÁ, Jana; Aleš HRDLIČKA; Jitka HEGROVÁ; Martina BUCKOVÁ; David PROCHAZKA; Pavel POŘÍZKA; Viktor KANICKÝ a Jozef KAISER

Vydání

Spectrochimica Acta Part B: Atomic Spectroscopy, Amsterdam, Elsevier, 2024, 0584-8547

Další údaje

Jazyk

angličtina

Typ výsledku

Článek v odborném periodiku

Obor

10406 Analytical chemistry

Stát vydavatele

Nizozemské království

Utajení

není předmětem státního či obchodního tajemství

Odkazy

URL

Impakt faktor

Impact factor: 3.800

Označené pro přenos do RIV

Ano

Kód RIV

RIV/00216224:14310/24:00135573

Organizační jednotka

Přírodovědecká fakulta

Klíčová slova česky

spektroskopie laserem buzeného plazmatu (LIBS); filtr, řasy; optimalizace; diagnostika plazmatu

Klíčová slova anglicky

Laser-induced breakdown spectroscopy; Algae; Filter; Optimization; Plasma diagnostics

Štítky

14313010, rivok

Příznaky

Mezinárodní význam, Recenzováno

Změněno: 4. 4. 2025 12:40, Mgr. Marie Novosadová Šípková, DiS.

Anotace

V originále

The nickel and zinc contamination of algae on a cellulose filter was studied with double pulse 1064–1064 nm laser-induced breakdown spectroscopy (LIBS). Samples of the green alga Desmodesmus subspicatus were contaminated with zinc and nickel. The surface concentrations on the filter calculated from the reference Inductively Coupled Plasma Mass Spectrometry analysis were 25 and 64 ng cm−2 for nickel and zinc respectively. The algae are resting on the filter after drying and a double adhesive tape was used to fix the sample on the microscopic glass. During optimization method a compromise of 23–30 mJ pulse energies were set for maintaining a detectable or highest signal intensity of the analyte and not destroying the filter. Best conditions for maximum analyte signal and minimum deviation between the spectral behaviour of the analyte and the compared line of Na I, K I, Mg I, Mg II, Mn I, Mn II, Ca I, Ca II, and C I was 700 ns gate delay and 0 s interpulse delay. The deviation was rather more influenced with the signal-to-noise ratio of the analyte line than the closeness of the upper-level energies of the compared lines. The filter without algae showed systematically lower electron number density and total emissivity by units of percents than the filter with algae.

Návaznosti

MUNI/A/1298/2022, interní kód MU

Název: Základní a aplikovaný výzkum a vývoj metod chemické a fyzikálně chemické analýzy pro studium přírody a pokročilé technologie

Investor: Masarykova univerzita, Základní a aplikovaný výzkum a vývoj metod chemické a fyzikálně chemické analýzy pro studium přírody a pokročilé technologie

Citovat

HORSKÁ, Jana; Aleš HRDLIČKA; Jitka HEGROVÁ; Martina BUCKOVÁ; David PROCHAZKA; Pavel POŘÍZKA; Viktor KANICKÝ a Jozef KAISER. Study of spectral lines behaviour with a double pulse 1064–1064 nm laser-induced breakdown spectroscopy system at the direct analysis of algae on the filter. Spectrochimica Acta Part B: Atomic Spectroscopy. Amsterdam: Elsevier, 2024, roč. 213, March 2024, s. 1-8. ISSN 0584-8547. Dostupné z: https://doi.org/10.1016/j.sab.2024.106883.

@article{2378699,
   author = {Horská, Jana and Hrdlička, Aleš and Hegrová, Jitka and Bucková, Martina and Prochazka, David and Pořízka, Pavel and Kanický, Viktor and Kaiser, Jozef},
   article_location = {Amsterdam},
   article_number = {March 2024},
   doi = {https://doi.org/10.1016/j.sab.2024.106883},
   keywords = {Laser-induced breakdown spectroscopy; Algae; Filter; Optimization; Plasma diagnostics},
   language = {eng},
   issn = {0584-8547},
   journal = {Spectrochimica Acta Part B: Atomic Spectroscopy},
   title = {Study of spectral lines behaviour with a double pulse 1064–1064 nm laser-induced breakdown spectroscopy system at the direct analysis of algae on the filter},
   url = {https://www.sciencedirect.com/science/article/pii/S0584854724000272},
   volume = {213},
   year = {2024}
}

TY  - JOUR
ID  - 2378699
AU  - Horská, Jana - Hrdlička, Aleš - Hegrová, Jitka - Bucková, Martina - Prochazka, David - Pořízka, Pavel - Kanický, Viktor - Kaiser, Jozef
PY  - 2024
TI  - Study of spectral lines behaviour with a double pulse 1064–1064 nm laser-induced breakdown spectroscopy system at the direct analysis of algae on the filter
JF  - Spectrochimica Acta Part B: Atomic Spectroscopy
VL  - 213
IS  - March 2024
SP  - 1-8
EP  - 1-8
PB  - Elsevier
SN  - 05848547
KW  - Laser-induced breakdown spectroscopy
KW  - Algae
KW  - Filter
KW  - Optimization
KW  - Plasma diagnostics
UR  - https://www.sciencedirect.com/science/article/pii/S0584854724000272
N2  - The nickel and zinc contamination of algae on a cellulose filter was studied with double pulse 1064–1064 nm laser-induced breakdown spectroscopy (LIBS). Samples of the green alga Desmodesmus subspicatus were contaminated with zinc and nickel. The surface concentrations on the filter calculated from the reference Inductively Coupled Plasma Mass Spectrometry analysis were 25 and 64 ng cm−2 for nickel and zinc respectively. The algae are resting on the filter after drying and a double adhesive tape was used to fix the sample on the microscopic glass. During optimization method a compromise of 23–30 mJ pulse energies were set for maintaining a detectable or highest signal intensity of the analyte and not destroying the filter. Best conditions for maximum analyte signal and minimum deviation between the spectral behaviour of the analyte and the compared line of Na I, K I, Mg I, Mg II, Mn I, Mn II, Ca I, Ca II, and C I was 700 ns gate delay and 0 s interpulse delay. The deviation was rather more influenced with the signal-to-noise ratio of the analyte line than the closeness of the upper-level energies of the compared lines. The filter without algae showed systematically lower electron number density and total emissivity by units of percents than the filter with algae.
ER  -

HORSKÁ, Jana; Aleš HRDLIČKA; Jitka HEGROVÁ; Martina BUCKOVÁ; David PROCHAZKA; Pavel POŘÍZKA; Viktor KANICKÝ a Jozef KAISER. Study of spectral lines behaviour with a double pulse 1064–1064 nm laser-induced breakdown spectroscopy system at the direct analysis of algae on the filter. \textit{Spectrochimica Acta Part B: Atomic Spectroscopy}. Amsterdam: Elsevier, 2024, roč.~213, March 2024, s.~1-8. ISSN~0584-8547. Dostupné z: https://doi.org/10.1016/j.sab.2024.106883.

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