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@article{2388080,
author = {Crha, Tomáš and Odedina, Grace F and Pazourek, Jiří},
article_location = {BASEL},
article_number = {2},
doi = {http://dx.doi.org/10.3390/separations11020045},
keywords = {HILIC; ELSD; saccharides; sugar alcohols; isomaltulose (Palatinose); food supplements},
language = {eng},
issn = {1541-9290},
journal = {Fluid - Particle Separations Journal},
title = {HILIC Separation Methods on Poly-Hydroxyl Stationary Phases for Determination of Common Saccharides with Evaporative Light-Scattering Detector and Rapid Determination of Isomaltulose in Protein-Rich Food Supplements},
url = {https://www.mdpi.com/2297-8739/11/2/45},
volume = {11},
year = {2024}
}
TY - JOUR
ID - 2388080
AU - Crha, Tomáš - Odedina, Grace F - Pazourek, Jiří
PY - 2024
TI - HILIC Separation Methods on Poly-Hydroxyl Stationary Phases for Determination of Common Saccharides with Evaporative Light-Scattering Detector and Rapid Determination of Isomaltulose in Protein-Rich Food Supplements
JF - Fluid - Particle Separations Journal
VL - 11
IS - 2
SP - 1-16
EP - 1-16
PB - American Filtration and Separations Society
SN - 15419290
KW - HILIC
KW - ELSD
KW - saccharides
KW - sugar alcohols
KW - isomaltulose (Palatinose)
KW - food supplements
UR - https://www.mdpi.com/2297-8739/11/2/45
N2 - This article highlights the fundamental aspects of hydrophilic interaction liquid chromatography (HILIC) on poly-hydroxyl stationary phases to analyze non-derivatized mono- and disaccharides, including commonly consumed carbohydrates like glucose, fructose, sucrose, and lactose. The evaporative light-scattering detector (ELSD) is utilized as an alternative to an MS detector, and the separation system's selectivity allows the separation of anomers of monosaccharides. The study also includes a rapid method for determining isomaltulose (Palatinose), which was validated and applied to food supplement samples available in the Czech market, even those with high protein content. Additionally, isomaltulose was separated from sucrose in just 13 min.
ER -
CRHA, Tomáš, Grace F ODEDINA a Jiří PAZOUREK. HILIC Separation Methods on Poly-Hydroxyl Stationary Phases for Determination of Common Saccharides with Evaporative Light-Scattering Detector and Rapid Determination of Isomaltulose in Protein-Rich Food Supplements. \textit{Fluid - Particle Separations Journal}. BASEL: American Filtration and Separations Society, 2024, roč.~11, č.~2, s.~1-16. ISSN~1541-9290. Dostupné z: https://dx.doi.org/10.3390/separations11020045.
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