Low-Temperature Synthesis of GeTe Nanoparticles

J 2024

Low-Temperature Synthesis of GeTe Nanoparticles

BOUSKA, Marek; Yaraslava MILASHEUSKAYA; Miroslav SLOUF; Petr KNOTEK; Stanislav PECHEV et al.

Základní údaje

Originální název

Low-Temperature Synthesis of GeTe Nanoparticles

Autoři

BOUSKA, Marek; Yaraslava MILASHEUSKAYA; Miroslav SLOUF; Petr KNOTEK; Stanislav PECHEV; Lubomír PROKEŠ; Lukáš PEČINKA; Josef HAVEL; Miroslav NOVAK; Roman JAMBOR a Petr NEMEC

Vydání

Chemistry - A European Journal, Weinheim, WILEY- VCH VERLAG GMBH, 2024, 0947-6539

Další údaje

Jazyk

angličtina

Typ výsledku

Článek v odborném periodiku

Obor

10400 1.4 Chemical sciences

Stát vydavatele

Německo

Utajení

není předmětem státního či obchodního tajemství

Odkazy

URL

Impakt faktor

Impact factor: 3.700

Označené pro přenos do RIV

Ano

Kód RIV

RIV/00216224:14310/24:00137657

Organizační jednotka

Přírodovědecká fakulta

Klíčová slova anglicky

Nanoparticles; Chalcogenides; GeTe; Organometallic precursor

Štítky

14313010, rivok

Příznaky

Mezinárodní význam, Recenzováno

Změněno: 9. 2. 2025 18:45, Mgr. Pavla Foltynová, Ph.D.

Anotace

V originále

Nanoparticles can offer an alternative approach to fabricate phase-change materials. The chemical synthesis of GeTe nanoparticles using organometallic precursors exploits high-boiling solvents and relatively high temperatures (close or even above crystallization temperatures), as reported in the available literature. The aim of this work is the preparation of GeTe nanoparticles by a low-temperature synthetic method exploiting new organometallic precursors and common organic solvents. Indeed, different preparation methods and characterization of GeTe nanoparticles is discussed. The characterization of the prepared nanomaterial was performed on the basis of X-ray diffraction, transmission electron microscopy, scanning electron microscopy with energy dispersive X-ray spectroscopy, laser ablation time-of-flight mass spectrometry, Raman scattering spectroscopy, and dynamic light scattering. The results show that the low-temperature synthetic route leads to amorphous GeTe nanoparticles. Exploited organometallic precursor is stabilised by neutral ligand which can be isolated after the reaction and repeatedly used for further reactions. Furthermore, GeTe nanoparticle size can be tuned by the conditions of the synthesis.

Návaznosti

GA22-07635S, projekt VaV

Název: Pokročilé metody přípravy telluridů polokovů a nepřechodných kovů

Investor: Grantová agentura ČR, Pokročilé metody přípravy telluridů polokovů a nepřechodných kovů

Citovat

BOUSKA, Marek; Yaraslava MILASHEUSKAYA; Miroslav SLOUF; Petr KNOTEK; Stanislav PECHEV; Lubomír PROKEŠ; Lukáš PEČINKA; Josef HAVEL; Miroslav NOVAK; Roman JAMBOR a Petr NEMEC. Low-Temperature Synthesis of GeTe Nanoparticles. Chemistry - A European Journal. Weinheim: WILEY- VCH VERLAG GMBH, 2024, roč. 30, č. 61, s. 1-8. ISSN 0947-6539. Dostupné z: https://doi.org/10.1002/chem.202402319.

@article{2452076,
   author = {Bouska, Marek and Milasheuskaya, Yaraslava and Slouf, Miroslav and Knotek, Petr and Pechev, Stanislav and Prokeš, Lubomír and Pečinka, Lukáš and Havel, Josef and Novak, Miroslav and Jambor, Roman and Nemec, Petr},
   article_location = {Weinheim},
   article_number = {61},
   doi = {https://doi.org/10.1002/chem.202402319},
   keywords = {Nanoparticles; Chalcogenides; GeTe; Organometallic precursor},
   language = {eng},
   issn = {0947-6539},
   journal = {Chemistry - A European Journal},
   title = {Low-Temperature Synthesis of GeTe Nanoparticles},
   url = {https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/chem.202402319},
   volume = {30},
   year = {2024}
}

TY  - JOUR
ID  - 2452076
AU  - Bouska, Marek - Milasheuskaya, Yaraslava - Slouf, Miroslav - Knotek, Petr - Pechev, Stanislav - Prokeš, Lubomír - Pečinka, Lukáš - Havel, Josef - Novak, Miroslav - Jambor, Roman - Nemec, Petr
PY  - 2024
TI  - Low-Temperature Synthesis of GeTe Nanoparticles
JF  - Chemistry - A European Journal
VL  - 30
IS  - 61
SP  - 1-8
EP  - 1-8
PB  - WILEY- VCH VERLAG GMBH
SN  - 09476539
KW  - Nanoparticles
KW  - Chalcogenides
KW  - GeTe
KW  - Organometallic precursor
UR  - https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/chem.202402319
N2  - Nanoparticles can offer an alternative approach to fabricate phase-change materials. The chemical synthesis of GeTe nanoparticles using organometallic precursors exploits high-boiling solvents and relatively high temperatures (close or even above crystallization temperatures), as reported in the available literature. The aim of this work is the preparation of GeTe nanoparticles by a low-temperature synthetic method exploiting new organometallic precursors and common organic solvents. Indeed, different preparation methods and characterization of GeTe nanoparticles is discussed. The characterization of the prepared nanomaterial was performed on the basis of X-ray diffraction, transmission electron microscopy, scanning electron microscopy with energy dispersive X-ray spectroscopy, laser ablation time-of-flight mass spectrometry, Raman scattering spectroscopy, and dynamic light scattering. The results show that the low-temperature synthetic route leads to amorphous GeTe nanoparticles. Exploited organometallic precursor is stabilised by neutral ligand which can be isolated after the reaction and repeatedly used for further reactions. Furthermore, GeTe nanoparticle size can be tuned by the conditions of the synthesis.
ER  -

BOUSKA, Marek; Yaraslava MILASHEUSKAYA; Miroslav SLOUF; Petr KNOTEK; Stanislav PECHEV; Lubomír PROKEŠ; Lukáš PEČINKA; Josef HAVEL; Miroslav NOVAK; Roman JAMBOR a Petr NEMEC. Low-Temperature Synthesis of GeTe Nanoparticles. \textit{Chemistry - A European Journal}. Weinheim: WILEY- VCH VERLAG GMBH, 2024, roč.~30, č.~61, s.~1-8. ISSN~0947-6539. Dostupné z: https://doi.org/10.1002/chem.202402319.

Přehled o publikaci