| ŽÍDEK, Lukáš, Haihong WU, Juli FEIGON a Vladimír SKLENÁŘ. Measurement of small scalar and resiudal dipolar couplings in purine and pyrimidine bases. Journal of Biomolecular NMR. Dordrecht: Kluwer/Escom, 2001, roč. 21, č. 2, s. 153-159. ISSN 0925-2738. |
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@article{375591,
author = {Žídek, Lukáš and Wu, Haihong and Feigon, Juli and Sklenář, Vladimír},
article_location = {Dordrecht},
article_number = {2},
keywords = {NMR methods; nucleic acid bases; residual dipolar couplings; spin-state-selective filter},
language = {eng},
issn = {0925-2738},
journal = {Journal of Biomolecular NMR},
title = {Measurement of small scalar and resiudal dipolar couplings in purine and pyrimidine bases},
volume = {21},
year = {2001}
}
TY - JOUR
ID - 375591
AU - Žídek, Lukáš - Wu, Haihong - Feigon, Juli - Sklenář, Vladimír
PY - 2001
TI - Measurement of small scalar and resiudal dipolar couplings in purine and pyrimidine bases
JF - Journal of Biomolecular NMR
VL - 21
IS - 2
SP - 153
EP - 153
PB - Kluwer/Escom
SN - 09252738
KW - NMR methods
KW - nucleic acid bases
KW - residual dipolar couplings
KW - spin-state-selective filter
N2 - A suite of spin-state-selective excitation (S3E) NMR experiments for the measurements of small one-bond (13C - 13C, 13C - 15N) and two-bond (1H - 13C, 1H - 15N) coupling constants in 13C, 15N labeled purine and pyrimidine bases is presented. The incorporation of band-selective shaped pulses, elimination of the cross talk between á and â sub-spectra, and accuracy and precision of the proposed approach are discussed. Merits of using S3 E rather than á/â-half-filter are demonstrated using results obtained on isotopicaly labeled DNA oligonucleotides.
ER -
ŽÍDEK, Lukáš, Haihong WU, Juli FEIGON a Vladimír SKLENÁŘ. Measurement of small scalar and resiudal dipolar couplings in purine and pyrimidine bases. \textit{Journal of Biomolecular NMR}. Dordrecht: Kluwer/Escom, 2001, roč.~21, č.~2, s.~153-159. ISSN~0925-2738.
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