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@article{562524,
author = {Ahmed, M. and Schwendt, P. and Sivák, M. and Marek, Jaromír},
article_location = {Netherlands},
article_number = {6},
keywords = {Peroxovanadium(V); X-ray structure; NMR; hydroxyhippuric acid},
language = {eng},
issn = {0340-4285},
journal = {Transition Metal Chemistry},
title = {Synthesis and characterization of vanadium(V) complexes with alpha-hydroxyhippuric acid. The X-ray crystal structure of (NBu4)2[V2O2(O2)2(R-alpha-hhip) (S--hhip)].5H2O,[alpha-hhip = alpha-hydroxyhippurato(2-)]},
volume = {29},
year = {2004}
}
TY - JOUR
ID - 562524
AU - Ahmed, M. - Schwendt, P. - Sivák, M. - Marek, Jaromír
PY - 2004
TI - Synthesis and characterization of vanadium(V) complexes with alpha-hydroxyhippuric acid. The X-ray crystal structure of (NBu4)2[V2O2(O2)2(R-alpha-hhip) (S--hhip)].5H2O,[alpha-hhip = alpha-hydroxyhippurato(2-)]
JF - Transition Metal Chemistry
VL - 29
IS - 6
SP - 675-680
EP - 675-680
PB - Kluwer Academic Publishers
SN - 03404285
KW - Peroxovanadium(V)
KW - X-ray structure
KW - NMR
KW - hydroxyhippuric acid
N2 - Peroxovanadium(V) complexes of alpha-hydroxyhippuric acid (alpha-H2hhip), M2[V2O2(O2)2(alpha-hhip)2].nH2O, [M=K+(1), NH4+(2), NEt4+(3), NBu4+(4); n=5.5, 3, 8, 5) have been prepared and characterized by elemental analysis, i.r., u.v.-vis. and 51V-n.m.r. spectroscopies and by thermal analysis. The X-ray structure determination of (4) revealed the presence of dinuclear [V2O2(O2)2(R-alpha-hhip)(S-alpha-hhip)]2- anions with a planar V2O2 bridging core and seven-coordinated central atoms. The coordination geometry of the vanadium atom is a distorted pentagonal bipyramid.
ER -
AHMED, M., P. SCHWENDT, M. SIVÁK a Jaromír MAREK. Synthesis and characterization of vanadium(V) complexes with alpha-hydroxyhippuric acid. The X-ray crystal structure of (NBu4)2[V2O2(O2)2(R-alpha-hhip) (S--hhip)].5H2O,[alpha-hhip = alpha-hydroxyhippurato(2-)]. \textit{Transition Metal Chemistry}. Netherlands: Kluwer Academic Publishers, 2004, roč.~29, č.~6, s.~675-680. ISSN~0340-4285.
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